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Perkin Transactions 1 1972-2002 logo

Year 1995
Main Index

Issue 1


Front cover

pg X001; DOI:
10.1039/P199500FX001
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Contents pages

pg P001; DOI:
10.1039/P199500FP001
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(R)-(+)-3-Amino-2-phenylpropanoic acid: a revised absolute configuration based on an enantioselective synthesis and an X-ray crystal structure of the salt with (1S)-(+)-camphor-10-sulfonic acid
Alice A. D'Souza Majid Motevalli Andrew J. Robinson and Peter B. Wyatt
pg 1; DOI:
10.1039/P19950000001
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Platinum-catalysed addition of trimethylgermane to 1-trimethylsilylalk-1-ynes: a convenient synthesis of functionalised 2-trimethylgermylalk-1-enes
Edward Piers and René Lemieux
pg 3; DOI:
10.1039/P19950000003
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Back cover

pg X003; DOI:
10.1039/P199500BX003
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Nickel-catalysed substitutions of aryl tert-butyl sulfones with organometallic reagents: synthesis of ortho-substituted unsymmetrical biaryls
Jonathan Clayden J. Jonathan A. Cooney and Marc Julia
pg 7; DOI:
10.1039/P19950000007
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Improved synthesis of isoguanosine and 6-substituted xanthosine derivatives
Lorenzo De Napoli Daniela Montesarchio Gennaro Piccialli Ciro Santacroce and Michela Varra
pg 15; DOI:
10.1039/P19950000015
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Radical cyclisation in heterocycle synthesis. Part 1. Sulfanyl radical addition–cyclisation of dienylamides for lactam synthesis
Takeaki Naito Yuko Honda Okiko Miyata and Ichiya Ninomiya
pg 19; DOI:
10.1039/P19950000019
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(Halogenomethyl)phenyl -D-glucopyranosides as enzyme-activated irreversible inhibitors of yeast -glucosidase and potential anti-HIV agents
Josie C. Briggs Alan H. Haines and Richard J. K. Taylor
pg 27; DOI:
10.1039/P19950000027
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Additivity relationships in the carbon-13 nuclear magnetic resonance spectra of polyhydroxy steroids
Masaru Kobayashi
pg 33; DOI:
10.1039/P19950000033
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[3 + 2] Cycloadditions of carbonyl oxides to imines: an alternative approach to the synthesis of 1,2,4-dioxazolidines
Kevin J. McCullough Mitsuyuki Mori Toshihiko Tabuchi Hideyuki Yamakoshi Shigekazu Kusabayashi and Masatomo Nojima
pg 41; DOI:
10.1039/P19950000041
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Photoinduced molecular transformations. Part 152. Ring expansion based on a sensitized [2 + 2] photoaddition of enol ethers of cyclic ketones with olefins, followed by a -scission of alkoxyl radicals generated from the resulting cyclobutanols. Two-carbon ring expansion of -indanone, -tetralone and -suberone
Hiroshi Suginome Toshihiro Takeda Masahito Itoh Yutaka Nakayama and Kazuhiro Kobayashi
pg 49; DOI:
10.1039/P19950000049
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Photoinduced molecular transformations. Part 153. Long-range intramolecular hydroxylation of C(25) of the cholestane side chain
Kazuhiko Orito Shinji Sato and Hiroshi Suginome
pg 63; DOI:
10.1039/P19950000063
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Photoinduced molecular transformations. Part 155. General synthesis of macrocyclic ketones based on a ring expansion involving a selective -scission of alkoxyl radicals, its application to a new synthesis of ()-isocaryophyllene and ()-caryophyllene, and a conformational analysis of the two sesquiterpenes and the radical intermediate in the synthesis by MM3 calculations
Hiroshi Suginome Takahiko Kondoh Camelia Gogonea Vishwakarma Singh Hitoshi Got and Eiji sawa
pg 69; DOI:
10.1039/P19950000069
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Design and synthesis of new bile acid-based macrocycles
Uday Maitra and S. Balasubramanian
pg 83; DOI:
10.1039/P19950000083
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Instructions for authors (1995)

pg vii; DOI:
10.1039/P19950000vii
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IUPAC publications on nomenclature and symbolism

pg xxv; DOI:
10.1039/P19950000xxv
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Conference diary

pg xxxi; DOI:
10.1039/P1995000xxxi
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Issue 2


Front cover

pg X005; DOI:
10.1039/P199500FX005
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Back cover

pg X007; DOI:
10.1039/P199500BX007
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Contents pages

pg P009; DOI:
10.1039/P199500FP009
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Back matter

pg P017; DOI:
10.1039/P199500BP017
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Lipase-catalysed Baeyer–Villiger reactions
Stephanie C. Lemoult Paul F. Richardson and Stanley M. Roberts
pg 89; DOI:
10.1039/P19950000089
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A convenient and general synthesis of alkanediyl diphenols
Cordula Grüttner Volker Böhmer Rosemarie Assmus and Sabine Scherf
pg 93; DOI:
10.1039/P19950000093
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Synthesis of acyl(phenylselanyl)methylidene(triphenyl)-5-arsanes and their Wittig-type reactions
Zhi-Zhen Huang Xian Huang and Yao-Zeng Huang
pg 95; DOI:
10.1039/P19950000095
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Synthetic applications of arenetricarbonylchromium(0) complexes: the synthesis of polyfunctionalised thiophenes
Michael S. Loft Timothy J. Mowlem and David A. Widdowson
pg 97; DOI:
10.1039/P19950000097
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Enhanced lability of -silyl groups in thiophenetricarbonylchromium(0) complexes
Michael S. Loft Timothy J. Mowlem David A. Widdowson and David J. Williams
pg 105; DOI:
10.1039/P19950000105
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Asymmetric synthesis of (1R,1R)- and (1S,1S)-bis(1-arylethyl)amines by way of a diastereoselective addition to chiral imines and oxaxolidines with organometallic reagents
Kimio Higashiyama Hiroaki Inoue Takayasu Yamauchi and Hiroshi Takahashi
pg 111; DOI:
10.1039/P19950000111
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Optical resolution and absolute stereochemistry of trans-2,5-dimethyl-1-phenyl-1-silacyclopentane
Hai-Shan Dang Brian P. Roberts and Derek A. Tocher
pg 117; DOI:
10.1039/P19950000117
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Effect of molecular sieves on the formation and acid-catalysed mono- and bis-cyclization of N-arylimines: easy entry to polycyclic ring systems by a novel cascade reaction
Oliver Temme and Sabine Laschat
pg 125; DOI:
10.1039/P19950000125
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5,9-Methanobenzoannulenamines. Part 1. Improved synthesis of 11-amino-5,9-methanobenzo[8]annulenes
Iain M. Gilbert (the late) Colin L. Hewett Duncan R. Rae James Redpath (the late) David S. Savage and Thomas Sleigh
pg 133; DOI:
10.1039/P19950000133
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Stereocontrol in the nucleophilic epoxidation of -(1-hydroxyalkyl)-,-unsaturated sulfones
Richard F. W. Jackson Stephen P. Standen William Clegg and Andrew McCamley
pg 141; DOI:
10.1039/P19950000141
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Control of diastereofacial selectivity in the nucleophilic epoxidation of -oxygenated ,-unsaturated sulfones
Richard F. W. Jackson Stephen P. Standen and William Clegg
pg 149; DOI:
10.1039/P19950000149
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Stereospecific synthesis of -deuteriated -amino acids: regiospecific deuteriation of chiral 3-isopropyl-2,5-dimethoxy-3,6-dihydropyrazines
Janet E. Rose Paul D. Leeson and David Gani
pg 157; DOI:
10.1039/P19950000157
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Carotenoids and related polyenes. Part 2. Photoisomerization of an allenic carotenoid, peridinin, and allenic model compounds
Yumiko Yamano Sanae Sumiya and Masayoshi Ito
pg 167; DOI:
10.1039/P19950000167
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On the mechanism for the phototransformation of 3-alkoxy-2-(2-furyl)-4-oxo-4H-1-benzopyrans
Satish C. Gupta Ashok Saini Devinder Kumar Narender S. Yadav Kuldeep Chand Satbir Mor and Som N. Dhawan
pg 177; DOI:
10.1039/P19950000177
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Corrigenda
Brindaban C. Ranu Manika Saha Sanjay Bhar R. Rathore J. S. Kim and J. K. Kochi
pg 183; DOI:
10.1039/P19950000183
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Conference diary

pg viia; DOI:
10.1039/P1995000viia
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Issue 3


Front cover

pg X009; DOI:
10.1039/P199500FX009
PDF
Back cover

pg X011; DOI:
10.1039/P199500BX011
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Contents pages

pg P019; DOI:
10.1039/P199500FP019
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A superior procedure for generation of substituted benzyllithiums from the corresponding chlorides
Keith Smith and Duanjie Hou
pg 185; DOI:
10.1039/P19950000185
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Facile synthesis of dihydrofurans by the cerium(IV) ammonium nitrate mediated oxidative addition of 1,3-dicarbonyl compounds to cyclic and acyclic alkenes. Relative superiority over the manganese(III) acetate mediated process
Vijay Nair and Jessy Mathew
pg 187; DOI:
10.1039/P19950000187
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PbCl2/Ga bimetal redox system-mediated carbon–carbon bond formation reactions between carbonyl compounds and ethyl trichloroacetate and iodoacetonitrile
Xiao-Lin Zhang Ying Han Wen-Tian Tao and Yao-Zeng Huang
pg 189; DOI:
10.1039/P19950000189
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Synthesis of alkyl and aryl substituted buta-1,2,3-trienes
Hak-Fun Chow Xiao-Ping Cao and Man-Kit Leung
pg 193; DOI:
10.1039/P19950000193
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Studies of chromenes. Part 11. 3-Substitution of 7-methoxy-2,2-dimethylchroman-4-one without ring opening via 3-bromination
Robert K. Akuamoah Philip E. Brown Wafa Y. Marcus and John E. Steele
pg 197; DOI:
10.1039/P19950000197
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Azoniaazulenes. Part 7. Functionalisation of 10H-azepino[1,2-a]indoles
Gurnos Jones Michael W. Kempa Michael B. Hursthouse and K. Abdul Malik
pg 203; DOI:
10.1039/P19950000203
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Preparation and enantiomer recognition behaviour of azophenolic crown ethers containing cis-cyclohexane-1,2-diol as the chiral centre
Koichiro Naemura Sachiko Takeuchi Keiji Hirose Yoshito Tobe Takahiro Kaneda and Yoshiteru Sakata
pg 213; DOI:
10.1039/P19950000213
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Excitatory amino acids. Synthesis of (RS)-2-amino-3-(5-cyclopropyl-3-hydroxyisoxazol-4-yl)propionic acid, a new potent and specific AMPA receptor agonist
Niels Skjærbæk Bjarke Ebert Erik Falch Lotte Brehm and Povl Krogsgaard-Larsen
pg 221; DOI:
10.1039/P19950000221
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Short synthetic route to congeners of the undecose antibiotic herbicidin
John R. Bearder Mark L. Dewis and Donald A. Whiting
pg 227; DOI:
10.1039/P19950000227
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Facile construction of the 1-phenylnaphthyl skeleton via an ester-mediated nucleophilic aromatic substitution reaction. Applications to the synthesis of phenylnaphthalide lignans
Tetsutaro Hattori Hideyuki Tanaka Yoshikazu Okaishi and Sotaro Miyano
pg 235; DOI:
10.1039/P19950000235
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Preparation of N-hydroxyazoles by oxidation of azoles
Mikael Begtrup and Per Vedsø
pg 243; DOI:
10.1039/P19950000243
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Antitumour imidazotetrazines. Part 31. The synthesis of isotopically labelled temozolomide and a multinuclear (1H, 13C, 15N) magnetic resonance investigation of temozolomide and mitozolomide
Richard T. Wheelhouse Derry E. V. Wilman William Thomson and Malcolm F. G. Stevens
pg 249; DOI:
10.1039/P19950000249
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Reactions of tetrasulfur tetranitride with aryl dibromomethyl ketones: one-pot synthesis of 3-aroylformamido-4-aryl-1,2,5-thiadiazoles and their reactions
Kyongtae Kim Jaeeock Cho and Sung Cheol Yoon
pg 253; DOI:
10.1039/P19950000253
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Regioselectivity in the reductive cleavage of pyrogallol derivatives: reductive electrophilic substitution of acetals of 2,3-dimethoxyphenol
Ugo Azzena Giovanni Melloni and Luisa Pisano
pg 261; DOI:
10.1039/P19950000261
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Novel preparation of 3-alkyl-5-hydroxy-5-per(poly)fluoroalkyl-4,5-dihydroisoxazoles
Jian Chen and Chang-Ming Hu
pg 267; DOI:
10.1039/P19950000267
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Stereoselective radical additions of -oxy-,-unsaturated ester derivatives; 1,2-asymmetric induction in acyclic and cyclisation systems
Tsutomu Morikawa Yoshiaki Washio Susumu Harada Ryo Hanai Takashi Kayashita Hisako Nemoto Motoo Shiro and Takeo Taguchi
pg 271; DOI:
10.1039/P19950000271
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Conference diary

pg viib; DOI:
10.1039/P1995000viib
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Issue 4


Front cover

pg X013; DOI:
10.1039/P199500FX013
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Back cover

pg X015; DOI:
10.1039/P199500BX015
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Contents pages

pg P027; DOI:
10.1039/P199500FP027
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Back matter

pg P039; DOI:
10.1039/P199500BP039
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Proof that acetic acid is extruded during biosynthesis of vitamin B12 in Pseudomonas denitrificans
Yongfu Li N. Patrick J. Stamford and Alan R. Battersby
pg 283; DOI:
10.1039/P19950000283
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Diastereocontrol in the reaction of amide-homoenolates with aromatic aldehydes
Satoshi Sakami Takashi Houkawa Morio Asaoka and Hisashi Takei
pg 285; DOI:
10.1039/P19950000285
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Synthesis of 11C-labelled ketones via carbonylative coupling reactions using [11C]carbon monoxide
Yvonne Andersson and Bengt Långström
pg 287; DOI:
10.1039/P19950000287
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Nitration of nonactivated arenes with a ternary system NO–NO2–O2. Mechanistic implications of the Kyodai-nitration
Hitomi Suzuki and Tadashi Mori
pg 291; DOI:
10.1039/P19950000291
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Porphyrin–phenothiazine hybrid molecules: marked dependence of light induced nuclease activity on the linker moiety
Goverdhan Mehta Thota Sambaiah Bhaskar G. Maiya Mallena Sirish and Aparna Dattagupta
pg 295; DOI:
10.1039/P19950000295
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Synthesis and anti-HIV-1 activity of bis-ketol AZT monophosphates
Gerald F. Koser Yali Huang Kuanchiang Chen and Kim C. Calvo
pg 299; DOI:
10.1039/P19950000299
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Diastereoselectivity in the preparation of -silyl esters from -unsaturated esters and amides attached to chiral auxiliaries
Ian Fleming and Nicholas D. Kindon
pg 303; DOI:
10.1039/P19950000303
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The phenyldimethylsilyl group as a masked hydroxy group
Ian Fleming Rolf Henning David C. Parker Howard E. Plaut and Philip E. J. Sanderson
pg 317; DOI:
10.1039/P19950000317
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Ozone-mediated reaction of anilides and phenyl esters with nitrogen dioxide: enhanced ortho-reactivity and mechanistic implications
Hitomi Suzuki Atsuo Tatsumi Taro Ishibashi and Tadashi Mori
pg 339; DOI:
10.1039/P19950000339
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Some enantioselective borane reductions of prochiral ketones catalysed by polymer-supported oxazaborolidines bound via the boron atom
Claude Caze Noureddine El Moualij Philip Hodge Christopher J. Lock and Jianbiao Ma
pg 345; DOI:
10.1039/P19950000345
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Development of a synthesis of lankacidins: stereoselective synthesis of the -lactone fragment
Eric J. Thomas and Andrew C. Williams
pg 351; DOI:
10.1039/P19950000351
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Development of a synthesis of lankacidins: synthesis of the C(14)–C(6) fragment and introduction of the C(10)–C(13) diene
Jane M. Roe and Eric J. Thomas
pg 359; DOI:
10.1039/P19950000359
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Synthesis of 7-benzylideneoctahydro-2H-pyrido[1,2-a]pyrazines, bicyclic analogues of the calcium antagonist flunarizine
M. Ashty Saleh Frans Compernolle Suzanne Toppet and Georges J. Hoornaert
pg 369; DOI:
10.1039/P19950000369
PDF
Photochemical isomerization of O-allyl and O-but-3-enyl thiocarbamates
Masami Sakamoto Mitsuru Yoshiaki Masaki Takahashi Tsutomu Fujita and Shoji Watanabe
pg 373; DOI:
10.1039/P19950000373
PDF
Hydroxyl-directed reduction of -hydroxycycloalkanones as a stereoselective route to 1,3-diols: X-ray crystal structure and structural features of (1R*,2R*,6S*)-2-[hydroxy(phenyl)methyl]cyclopentanol
Stephen H. J. Thompson Mary F. Mahon Kieran C. Molloy Michael S. Hadley and Timothy Gallagher
pg 379; DOI:
10.1039/P19950000379
PDF
Synthesis of a derivative of triangulene; the first non-kekul polynuclear aromatic
Graeme Allinson Richard J. Bushby Jean-Louis Paillaud and Mark Thornton-Pett
pg 385; DOI:
10.1039/P19950000385
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Structure and relative stereochemistry of a new polycyclic alkaloid, asparagamine A, showing anti-oxytocin activity, isolated from Asparagus racemosus
Toshikazu Sekine Fumio Ikegami Nobuaki Fukasawa Yumi Kashiwagi Tatsuo Aizawa Yuichi Fujii Nijsiri Ruangrungsi and Isamu Murakoshi
pg 391; DOI:
10.1039/P19950000391
PDF
Synthesis of uridine derivatives containing strategically placed radical traps as potential inhibitors of ribonucleotide reductase
Sandra P. Auguste and Douglas W. Young
pg 395; DOI:
10.1039/P19950000395
PDF
Dithiasuccinoyl (Dts) amino-protecting group used in syntheses of 1,2-trans-amino sugar glycosides
Ernst Meinjohanns Morten Meldal Hans Paulsen and Klaus Bock
pg 405; DOI:
10.1039/P19950000405
PDF
Synthetic reactions of 2-(2-amino-3-cyano-4H-[1]benzopyran-4-yl)propane-1,3-dinitrile with reactive methylene compounds
Conor N. O'Callaghan T. Brian H. McMurry and John E. O'Brien
pg 417; DOI:
10.1039/P19950000417
PDF
Use of bis[2-(trialkylsilyl)ethyl]N,N-dialkylphosphoramidites for the synthesis of phosphate monoesters
Kenneth C. Ross Daniel L. Rathbone William Thomson and Sally Freeman
pg 421; DOI:
10.1039/P19950000421
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Asymmetric reduction of prochiral aromatic ketones by borane–amine complexes in the presence of chiral amine–BF3 catalysts
Mariappan Periasamy J. V. Bhaskar Kanth and Ch. Kishan Reddy
pg 427; DOI:
10.1039/P19950000427
PDF
Rearrangement of S-methylbenzylsulfonium S-alkylides in non-basic media
Tohru Tanzawa Miyuki Ichioka Naohiro Shirai and Yoshiro Sato
pg 431; DOI:
10.1039/P19950000431
PDF
Modification of cyclodextrins by insertion of a heterogeneous sugar unit into their skeletons. Synthesis of 2-amino-2-deoxy--cyclodextrin from -cyclodextrin
Nobuo Sakairi Lai-Xi Wang and Hiroyoshi Kuzuhara
pg 437; DOI:
10.1039/P19950000437
PDF
Quinolinone cycloaddition as a potential synthetic route to dimeric quinoline alkaloids
Stephen A. Barr Charles F. Neville (the late) Michael F. Grundon Derek R. Boyd John F. Malone and Timothy A. Evans
pg 445; DOI:
10.1039/P19950000445
PDF
Selective electrophilic additions of mixed bifunctionalized trimethylenemethane dianion synthons
George Majetich Hisaya Nishidie and Yong Zhang
pg 453; DOI:
10.1039/P19950000453
PDF
Photochemical reactions of o-alkenylphenols and 1-alkenyl-2-naphthol with alkylamines: amination via photoinduced proton transfer
Masahide Yasuda Tatsuya Sone Kimiko Tanabe and Kensuke Shima
pg 459; DOI:
10.1039/P19950000459
PDF
Synthesis of perhydro-1,4-ethano-1,5-naphthyridine and perhydro-4,7-ethanopyrrolo[3,2-b]pyridine derivatives: potential NK1-receptor antagonists. X-Ray molecular structures of (4aR,8S,8aR)-6-oxo-8-phenylperhydro-1,4-ethano-1,5-naphthyridine and (4aR,7R,8R,8aR)-7,8-diphenylperhydro-1,4-ethano-1,5-naphthyridine
Yevgeny Besidsky Kristina Luthman Alf Claesson Christopher J. Fowler Ingeborg Csöregh and Uli Hacksell
pg 465; DOI:
10.1039/P19950000465
PDF
Synthesis and reactivity of 6-carbamoyl-5-phenyl-2,3,5,6-tetrahydro-1H-1,4-ethanobenzo[f]quinoline. X-Ray molecular structure of (4aR,5S,6R,10bR)-5-phenyl-2,3,4a,5,6,10b-hexahydro-1H-1,4-ethanobenzo[f]quinolin-6-yl acetate
Yevgeny Besidsky Kristina Luthman Alf Claesson Ingeborg Csöregh and Uli Hacksell
pg 475; DOI:
10.1039/P19950000475
PDF
The biosynthesis of hyoscyamine: the process by which littorine rearranges to hyoscyamine
Richard J. Robins Nicola C. J. E. Chesters David O'Hagan Adrian J. Parr Nicholas J. Walton and Jack G. Woolley
pg 481; DOI:
10.1039/P19950000481
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The biosynthesis of tropic acid. Part 6. Enantioselective, intact incorporation of (R)-(+)-3-phenyllactic acid into the tropic acid ester alkaloids of Datura
Morteza Ansarin and Jack G. Woolley
pg 487; DOI:
10.1039/P19950000487
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Acylation of aldo 1-pyrroline 1-oxides (4,5-dihydro-3H-pyrrole 1-oxides) and the oxidation of the resulting 3-acyloxy-1-pyrrolines (3-acyloxy-4,5-dihydro-3H-pyrroles)
Neil J. Gibson and Alexander R. Forrester
pg 491; DOI:
10.1039/P19950000491
PDF
Preparation and the acid- and base-catalysed isomerisation of 5,5-dimethyl-3-phenyl-1-pyrroline 1-oxide (5,5-dimethyl-3-phenyl-4,5-dihydro-3H-pyrrole 1-oxide): unprecedented acid-catalysed 1,3-oxygen migration
Neil J. Gibson and Alexander R. Forrester
pg 501; DOI:
10.1039/P19950000501
PDF
Preparation and benzoylation of 3-hydroxy-2,3,5,5-tetramethyl-1-pyrroline 1-oxide (3-hydroxy-2,3,5,5-tetramethyl-4,5-dihydro-3H-pyrrole 1-oxide)
Neil J. Gibson Alexander R. Forrester and Charles Brown
pg 507; DOI:
10.1039/P19950000507
PDF
Reaction of noracronycine and 1-hydroxy-3-methoxy-10-methylacridone with alkyl- and aryl-lithiums: formation of quinone methides
Catherine Jolivet Christian Rivalle and Emile Bisagni
pg 511; DOI:
10.1039/P19950000511
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Conference diary

pg xi; DOI:
10.1039/P199500000xi
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Issue 5


Front cover

pg X017; DOI:
10.1039/P199500FX017
PDF
Back cover

pg X019; DOI:
10.1039/P199500BX019
PDF
Contents pages

pg P041; DOI:
10.1039/P199500FP041
PDF
Back matter

pg P049; DOI:
10.1039/P199500BP049
PDF
Synthesis of C-glycofuranosides by the stereoselective reduction of hemiacetals
Eguzkiñe Calzada Catherine A. Clarke Christine Roussin-Bouchard and Richard H. Wightman
pg 517; DOI:
10.1039/P19950000517
PDF
One-pot syntheses of 3-cyanoindoles from 3-acyl- and 3-ethoxycarbonyl-1,2-dihydrocinnoline-1,2-dicarboximides
Satoko Tanaka Kazuyoshi Seguchi and Akira Sera
pg 519; DOI:
10.1039/P19950000519
PDF
Synthesis of substructures of soraphen A: formation of the enolate of benzyl propionate
Bernard Loubinoux Jean-Luc Sinnes and Anthony C. O'Sullivan
pg 521; DOI:
10.1039/P19950000521
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Mechanistic studies of the palladium(II)–copper(II)-mediated demercuriation of cycloalkyl and cycloalkylmethyl systems
Adam P. Wells and William Kitching
pg 527; DOI:
10.1039/P19950000527
PDF
Synthesis and characterization of isomeric ,-bithienyls with -methylsulfanyl substituents
Ugo Folli Dario Iarossi Mauro Montorsi Adele Mucci and Luisa Schenetti
pg 537; DOI:
10.1039/P19950000537
PDF
The synthesis of precisely structured polyurethanes. Part 1. Monomer synthesis
Alistair A. Denholm Maurice H. George Helen C. Hailes Peter J. Tiffin and David A. Widdowson
pg 541; DOI:
10.1039/P19950000541
PDF
Selective alkylation and allylation of allylic halides by tetraorganoindates: regio- and stereo-selective synthesis of rosefuran and sesquirosefuran
Shuki Araki Shun-Ji Jin and Yasuo Butsugan
pg 549; DOI:
10.1039/P19950000549
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Chemo–enzymic synthesis of optically active ,-disubstituted -amino acids
Weiguo Liu Paul Ray and Steven A. Benezra
pg 553; DOI:
10.1039/P19950000553
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Photoreactions of 1,3-dihydroisobenzofuran-1-thiones and 1,3-dihydro-2-benzothiophene-1-thiones with alkenes
Takehiko Nishio
pg 561; DOI:
10.1039/P19950000561
PDF
Synthesis of 4-hydroxy-15-oxaandrost-4-en-3-one and other potential aromatase inhibitors from sandaracopimaric acid
M. Bordell Martín A. Fernández Mateos and R. Rubio González
pg 569; DOI:
10.1039/P19950000569
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Synthesis of water-soluble sugar derivatives of combretastatin A-4
Richard T. Brown Brian W. Fox John A. Hadfield Alan T. McGown Stephen P. Mayalarp George R. Pettit and Julie A. Woods
pg 577; DOI:
10.1039/P19950000577
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Constituents of Nothapodytes foetida
Angela Pirillo Luisella Verotta Pierluigi Gariboldi Elisabetta Torregiani and Ezio Bombardelli
pg 583; DOI:
10.1039/P19950000583
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Synthesis and Diels–Alder reactions of thioisobenzofurans
Jonathan H. Bailey Carolyn V. Coulter Andrew J. Pratt and Ward T. Robinson
pg 589; DOI:
10.1039/P19950000589
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Structure of conocephalenol, a sesquiterpenoid alcohol from the European liverwort Conocephalum conicum: determination of the absolute configuration by total synthesis
Motoo Tori Katsuyuki Nakashima Yoshinori Asakawa Joseph D. Connolly Leslie J. Harrison David S. Rycroft Jagdemba Singh and Neill Woods
pg 593; DOI:
10.1039/P19950000593
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Palladium complex-catalysed carbocyclization–distannylation, –disilylation and –silastannylation of bis-dienes using distannanes, disilanes and silylstannanes
Yasushi Obora Yasushi Tsuji Takeshi Kakehi Mitsunari Kobayashi Yoshihisa Shinkai Masahiro Ebihara and Takashi Kawamura
pg 599; DOI:
10.1039/P19950000599
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Conference diary

pg viic; DOI:
10.1039/P1995000viic
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Issue 6


Front cover

pg X021; DOI:
10.1039/P199500FX021
PDF
Back cover

pg X023; DOI:
10.1039/P199500BX023
PDF
Contents pages

pg P053; DOI:
10.1039/P199500FP053
PDF
SRN1 Synthesis of vic-dinitro compounds containing a nitrodioxane subunit
René Beugelmans Ali Amrollah Madjdabadi Tawfik Gharbaoui and (the late) André Lechevallier
pg 609; DOI:
10.1039/P19950000609
PDF
Synthesis and thermal reactivity of 2-azido-5-trimethylsilylthiophene and 2-azido-5-methylthiophene. The para-like substituent effect on fragmentation of the azido group
Darren Davies Piero Spagnolo and Paolo Zanirato
pg 613; DOI:
10.1039/P19950000613
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Rearrangement and cyclo--elimination of N-substituted amidines using (diacetoxyiodo)benzene
Christopher A. Ramsden and Helen L. Rose
pg 615; DOI:
10.1039/P19950000615
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A new catalytic transformation of diazo esters: hydride abstraction in dirhodium(II)-catalysed reactions
Michael P. Doyle Alexey B. Dyatkin and Christopher L. Autry
pg 619; DOI:
10.1039/P19950000619
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Tetrathiafulvalene: a catalyst for sequential radical–polar reactions
Rodney J. Fletcher Christopher Lampard John A. Murphy and Norman Lewis
pg 623; DOI:
10.1039/P19950000623
PDF
Low-temperature addition of hydrogen polysulfides to olefins: formation of 2,2-dialkyl polysulfides from alk-1-enes and cyclic (poly)sulfides and polymeric organic sulfur compounds from ,-dienes
Wim de Graaf Jaap S. Sinninghe Damsté and Jan W. de Leeuw
pg 635; DOI:
10.1039/P19950000635
PDF
Synthesis of the selective muscarinic agonist (3R)-3-(6-chloropyrazin-2-yl)-1-azabicyclo [2.2.2] octane
Michael S. Ashwood Andrew W. Gibson Peter G. Houghton Guy R. Humphrey D. Craig Roberts and Stanley H. B. Wright
pg 641; DOI:
10.1039/P19950000641
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Pigments of fungi. Part 40. Dermocanarins 1–3, unique naphthol- and naphthoquinone-anthraquinone dimers that contain a macrocyclic lactone ring from the fungus Dermocybe canaria Horak
Melvyn Gill and Alberto Giménez
pg 645; DOI:
10.1039/P19950000645
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Preparation of 2-chlorobuta-1,3-dienes by dichlorocyclopropanation of allylsilanes followed by desilylation
Michiharu Mitani Yosinori Kobayashi and Kikuhiko Koyama
pg 653; DOI:
10.1039/P19950000653
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Radio-iodinated gibberellin photoaffinity probes
Michael H. Beale Richard Hooley Mervyn J. Lewis Sally J. Smith and Jane L. Ward
pg 657; DOI:
10.1039/P19950000657
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Reaction of 4a-methyl-2,3,4,4a-tetrahydro-1H-carbazole with Grignard reagents
J. Gonzalo Rodríguez and Anahí Urrutia
pg 665; DOI:
10.1039/P19950000665
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Synthesis of [1,2,3-2,3-bis(benzyloxymethyl)cyclobutyl]imidazol-5-amines: important precursors to cyclobut-A derivatives
Brian L. Booth and Paul R. Eastwood
pg 669; DOI:
10.1039/P19950000669
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Two synthetic routes to 2,3-dideoxy-3-C-(hydroxymethyl)-4-thionucleosides
John Mann Allen J. Tench Alexander C. Weymouth-Wilson Sue Shaw-Ponter and Robert J. Young
pg 677; DOI:
10.1039/P19950000677
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Absolute stereochemistry of chinesin I and II
Yoshinori Aramaki Kazuhiro Chiba and Masahiro Tada
pg 683; DOI:
10.1039/P19950000683
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Samarium(II) diiodide-mediated intermolecular aldol type reactions of phenacyl bromides with carbonyl compounds
Yutaka Aoyagi Mizue Yoshimura Masako Tsuda Tomomasa Tsuchibuchi Saori Kawamata Hiroyuki Tateno Kazushi Asano Hiroko Nakamura Masako Obokata Akihiro Ohta and Yoshio Kodama
pg 689; DOI:
10.1039/P19950000689
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Synthesis of optically active azetidine-2,4-dicarboxylic acid and related chiral auxiliaries for asymmetric synthesis
Jun'ichi Hoshino Junko Hiraoka Yasuo Hata Seiji Sawada and Yukio Yamamoto
pg 693; DOI:
10.1039/P19950000693
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Oxidation of imines to oxaziridines catalysed by transition metal complexes using molecular oxygen as the terminal oxidant
Lars Martiny and Karl Anker Jørgensen
pg 699; DOI:
10.1039/P19950000699
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Synthesis and characterization of models for the bilin catabolites of chlorophylls using metallo--oxochlorins and -benzo[at]chlorins: comparison of macrocycle cleavage versus meso-oxochlorin formation
Meden Isaac Mathias O. Senge and Kevin M. Smith
pg 705; DOI:
10.1039/P19950000705
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Preparation and oxidative doping studies of dithienyl polyenes stabilized by alkyl group substitution
Charles W. Spangler and Mingqian He
pg 715; DOI:
10.1039/P19950000715
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Benzoannelated centropolyquinanes. Part 21. Centrohexaindane: three complementary syntheses of the highest member of the centropolyindane family
Dietmar Kuck Andreas Schuster Bernd Paisdor and Detlef Gestmann
pg 721; DOI:
10.1039/P19950000721
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Conference diary

pg viid; DOI:
10.1039/P1995000viid
PDF

Issue 7


Front cover

pg X025; DOI:
10.1039/P199500FX025
PDF
Back cover

pg X027; DOI:
10.1039/P199500BX027
PDF
Contents pages

pg P061; DOI:
10.1039/P199500FP061
PDF
Back matter

pg P071; DOI:
10.1039/P199500BP071
PDF
A new method for the synthesis of N-phenyl-uracil and -pyrimidine nucleosides
Tokumi Maruyama Keiichi Fujiwara and Mitsutoshi Fukuhara
pg 733; DOI:
10.1039/P19950000733
PDF
Highly selective asymmetric hydrolysis of 2,2-disubstituted epoxides using lyophilized cells of Rhodococcus sp. NCIMB 11216
Ute Wandel Martin Mischitz Wolfgang Kroutil and Kurt Faber
pg 735; DOI:
10.1039/P19950000735
PDF
Generation and reactions of butadienylthionium ions from 2-vinylcyclopropyl sulfoxides under Pummerer conditions
Tadashi Kataoka Harutoshi Matsumoto Tetsuo Iwama Taizo Ito and Hiroshi Shimizu
pg 737; DOI:
10.1039/P19950000737
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A new and convenient one-pot synthesis of ,-unsaturated trifluoromethyl ketones
Wei Sheng Huang and Cheng Ye Yuan
pg 741; DOI:
10.1039/P19950000741
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Synthesis and decomplexation of (-arene)(-cyclopentadienyl)-iron(II) hexafluorophosphates using microwave dielectric heating
Qumars Dabirmanesh Sharon I. S. Fernando and Roger M. G. Roberts
pg 743; DOI:
10.1039/P19950000743
PDF
A ketal Claisen rearrangement for -ketol isoprene unit elongation: application to a practical synthesis of sarcophytol A intermediate
Hisao Takayanagi Shigeo Sugiyama and Yasuhiro Morinaka
pg 751; DOI:
10.1039/P19950000751
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A total synthesis of an antibacterial clerodane, 16-hydroxycleroda-3,13(14)Z-dien-15,16-olide
Hisahiro Hagiwara Kazuhiro Inome and Hisashi Uda
pg 757; DOI:
10.1039/P19950000757
PDF
Structure of cereulide, a cyclic dodecadepsipeptide toxin from Bacillus cereus and studies on NMR characteristics of its alkali metal complexes including a conformational structure of the K+ complex
Sathorn Suwan Minoru Isobe Ikuko Ohtani Norio Agata Masashi Mori and Michio Ohta
pg 765; DOI:
10.1039/P19950000765
PDF
Total synthesis of (+)-compactin by a double Michael protocol
Hisahiro Hagiwara Takashi Nakano Masakazu Kon-no and Hisashi Uda
pg 777; DOI:
10.1039/P19950000777
PDF
Development of a synthesis of lankacidins: an investigation into 17-membered ring formation
Ernesto G. Mata and Eric J. Thomas
pg 785; DOI:
10.1039/P19950000785
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Adenine isosteres with bridgehead nitrogen. Part 1. Two independent syntheses of the [1,2,4]triazolo[1,5-a][1,3,5]triazine ring system leading to a range of substituents in the 2, 5 and 7 positions
Peter W. R. Caulkett Geraint Jones Mary McPartlin Nigel D. Renshaw Sarah K. Stewart and Brian Wright
pg 801; DOI:
10.1039/P19950000801
PDF
Mild thermal route to phthalimidonitrene and its reaction with activated benzenes to give 2H- and 3H-azepines; X-ray crystal structure analysis of an isolable 2H-azepine
David W. Jones and Mark Thornton-Pett
pg 809; DOI:
10.1039/P19950000809
PDF
An enantiospecific total synthesis of (+)-muricatacin
Peter Somfai
pg 817; DOI:
10.1039/P19950000817
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Synthesis and stereochemistry of optically active telluronium ylides
Nobumasa Kamigata Ayumi Matsuhisa Hideo Taka and Toshio Shimizu
pg 821; DOI:
10.1039/P19950000821
PDF
Selective ether cleavages: simple routes yielding di- and tri-functional hexaalkoxytriphenylenes
Fritz Closs Lukas Häußling Philippe Henderson Helmut Ringsdorf and Peter Schuhmacher
pg 829; DOI:
10.1039/P19950000829
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Synthesis based on cyclohexadienes. Part 17. Total synthesis of the sesquiterpenes of Eremophila georgei diels
Natesan Selvakumar Seenivasaga N. Janaki Kakumanu Pramod and G. S. R. Subba Rao
pg 839; DOI:
10.1039/P19950000839
PDF
Homochiral 2,3-epoxy sulfides—powerful new synthetic building blocks providing stereoselective access to 2,3-epoxy sulfoxides, 2,3-dihydroxy sulfoxides and (E)--hydroxy-,-unsaturated sulfoxides and sulfones. X-Ray molecular structure of rac-(2R*,3R*)-1-[(S*)-phenylsulfinyl] hexane-2,3-diol
Andrew D. Westwell Mark Thornton-Pett and Christopher M. Rayner
pg 847; DOI:
10.1039/P19950000847
PDF
Synthesis of bridged thiazolium salts as models for thiamin
Finian J. Leeper and David H. C. Smith
pg 861; DOI:
10.1039/P19950000861
PDF
Changes of enantioselectivity with the substrate ratio for the addition of diethylzinc to aldehydes using a catalyst coupled to a soluble polymer
Claus Dreisbach Gisela Wischnewski Udo Kragl and Christian Wandrey
pg 875; DOI:
10.1039/P19950000875
PDF
Free-radical cyclisations of 2-aminoalka-2,5-dienenitriles
Chau-Chen Yang and Jim-Min Fang
pg 879; DOI:
10.1039/P19950000879
PDF
Stereocontrolled synthesis of fluorosqualenes and fluoroepoxy-squalenes as inhibitors of squalene epoxidase and 2,3-oxidosqualene cyclase
Maurizio Ceruti Simona Amisano Paola Milla Franca Viola Flavio Rocco Michel Jung and Luigi Cattel
pg 889; DOI:
10.1039/P19950000889
PDF
Helically chiral thia- and diselena-quinquephenylophanes
Karri Airola Stefan Bartram and Kari Rissanen
pg 895; DOI:
10.1039/P19950000895
PDF
Syntheses of 2-ethyl-8-methyl-1,7-dioxaspiro[5.5]undecanols
Mark F. Jacobs Bill D. Suthers Achim Hübener and William Kitching
pg 901; DOI:
10.1039/P19950000901
PDF
Simple transphosphatidylation of phospholipids catalysed by a lipid-coated phospholipase D in organic solvents
Yoshio Okahata Ken-ichi Niikura and Kuniharu Ijiro
pg 919; DOI:
10.1039/P19950000919
PDF
Radical cyclisation route to furanolignans: short and stereoselective synthesis of ()-dihydrosesamin and ()-lariciresinol
Gourhari Maiti Sankar Adhikari and Subhas Chandra Roy
pg 927; DOI:
10.1039/P19950000927
PDF
Synthesis of 4,5,8-trimethoxy-9,10-dioxo-9,10-dihydroanthracene-2-carboxylic acid, an analogue of rhein with improved systemic exposure in the guinea pig
W. Martin Owton Michael Brunavs Martin V. Miles David R. Dobson and David J. Steggles
pg 931; DOI:
10.1039/P19950000931
PDF
Synthetic study of the highly potent and selective anti-platelet activating factor thiazolidin-4-one agents and related compounds
Yoo Tanabe Hitomi Yamamoto Masanari Murakami Kazunori Yanagi Yoshino Kubota Hitomi Okumura Yuzuru Sanemitsu and Gohfu Suzukamo
pg 935; DOI:
10.1039/P19950000935
PDF
Total synthesis of pterocarpan: ()-neorautenane
Ricardo A. Lichtenfels Antonio L. Coelho and Paulo R. R. Costa
pg 949; DOI:
10.1039/P19950000949
PDF
Synthesis of phenylalanine-based cyclic acylated enamino ester dipeptide analogues: inhibitors of -chymotrypsin. X-Ray molecular structure of (2S,4R)-4-benzyl-3-benzyloxycarbonyl-5-oxo-2-phenyloxazolidin-4-ylacetic acid
Andrew D. Abell Mark D. Oldham and Jane M. Taylor
pg 953; DOI:
10.1039/P19950000953
PDF
Conference diary

pg ix; DOI:
10.1039/P199500000ix
PDF

Issue 8


Front cover

pg X029; DOI:
10.1039/P199500FX029
PDF
Back cover

pg X031; DOI:
10.1039/P199500BX031
PDF
Contents pages

pg P081; DOI:
10.1039/P199500FP081
PDF
Back matter

pg P089; DOI:
10.1039/P199500BP089
PDF
Total synthesis of cis-clerodane diterpenoids: (–)-agelasine A and (+)-(3R,4S,5R,8S,9R,10S)-3,4-epoxyclerod-13-en-15,16-olide
Edward Piers M. Livain Breau Yongxin Han Guy L. Plourde and Wen-Lung Yeh
pg 963; DOI:
10.1039/P19950000963
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Enzymes in organic synthesis: oxidoreductions
Jim-Min Fang Chun-Hung Lin Curt W. Bradshaw and Chi-Huey Wong
pg 967; DOI:
10.1039/P19950000967
PDF
Nucleophilic addition of lithio derivatives to 1-substituted benzo[c][2,7]naphthyridines (2,9-diazaphenanthrenes)
Corinne Cochennec Patrick Rocca Francis Marsais Alain Godard and Guy Quéguiner
pg 979; DOI:
10.1039/P19950000979
PDF
Synthesis of 6,7- and 6,7-aziridinoandrost-4-ene-3,17-diones and related compounds: potential aromatase inhibitors
Vincent C. O. Njar Rolf W. Hartmann and Cecil H. Robinson
pg 985; DOI:
10.1039/P19950000985
PDF
Novel synthesis of trifluoromethylated allylic phosphonates
Yanchang Shen and Ming Qi
pg 993; DOI:
10.1039/P19950000993
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Synthesis of perfluoroalkylated heterocyclic phosphonates
Yanchang Shen Jianhua Zheng Yuankang Xin Yugang Lin and Ming Qi
pg 997; DOI:
10.1039/P19950000997
PDF
On the reactions of (vinylimino)phosphoranes and related compounds. Part 30. Short new synthesis of 5-azaazulene derivatives. Some comments on reactivities of (vinylimino)phosphoranes
Makoto Nitta Yukio Iino Satoshi Mori and Tohru Takayasu
pg 1001; DOI:
10.1039/P19950001001
PDF
1,2-Asymmetric induction in conjugate additions to nitroalkenes
Anthony G. M. Barrett and David J. Rys
pg 1009; DOI:
10.1039/P19950001009
PDF
Synthetic approaches to the angucycline antibiotics: the total syntheses of ()-rubiginone B1 and B2, ()-emycin A, and related analogues
David S. Larsen and Michael D. O'Shea
pg 1019; DOI:
10.1039/P19950001019
PDF
Regiospecific electrophilic substitution of aminoquinazolinones: directed lithiation of 3-(pivaloylamino)- and 3-(acetylamino)-2-methylquinazolin-4(3H)-ones
Keith Smith Gamal A. El-Hiti Mohamed A. Abdo and Mohamed F. Abdel-Megeed
pg 1029; DOI:
10.1039/P19950001029
PDF
A useful method for configurational assignment of vinyl sulfides; stereochemical reassessment of the radical addition of benzenethiol to alkynes
Luisa Benati Laura Capella Pier Carlo Montevecchi and Piero Spagnolo
pg 1035; DOI:
10.1039/P19950001035
PDF
Convenient and versatile synthesis of 3-(polyfluoroalkyl)pyrazoles
Xiao-Qing Tang and Chang-Ming Hu
pg 1039; DOI:
10.1039/P19950001039
PDF
Potential mechanism-based tyrosine kinase inhibitors. Part 1. Phosphorylation chemistry of pyridine N-oxides
David M. Andrews Timothy C. M. Page Josephine M. Peach and Andrew J. Pratt
pg 1045; DOI:
10.1039/P19950001045
PDF
Oligomeric isoflavonoids. Part 3. Daljanelins A–D, the first pterocarpan- and isoflavanoid-neoflavonoid analogues
J. Albert Ferreira Janetta W. Nel E. Vincent Brandt Barend C. B. Bezuidenhoudt and Daneel Ferreira
pg 1049; DOI:
10.1039/P19950001049
PDF
Catalytic oxidation of chlorpromazine and related phenothiazines. Cation radicals as the reactive intermediates in sulfoxide formation
Eric Bosch and Jay K. Kochi
pg 1057; DOI:
10.1039/P19950001057
PDF
Tandem sequence of ArSCl initiated AdE reactions resulting in formation of two C–C bonds
Irina P. Smoliakova Ron Caple Vincent R. Magnuson Valery R. Polyakov William A. Smit Alexander S. Shashkov and Bato D. Ohinov
pg 1065; DOI:
10.1039/P19950001065
PDF
Synthesis of the building blocks N-Fmoc-O-[-D-Ac3GalN3p-(1
Sandrine Rio-Anneheim Hans Paulsen Morten Meldal and Klaus Bock
pg 1071; DOI:
10.1039/P19950001071
PDF
Conference diary

pg viie; DOI:
10.1039/P1995000viie
PDF

Issue 9


Front cover

pg X033; DOI:
10.1039/P199500FX033
PDF
Journals bulletin

pg X035; DOI:
10.1039/P1995000X035
PDF
Back cover

pg X039; DOI:
10.1039/P199500BX039
PDF
Contents pages

pg P097; DOI:
10.1039/P199500FP097
PDF
Back matter

pg P105; DOI:
10.1039/P199500BP105
PDF
Potent inhibitor of the human rhinovirus (HRV) 3C protease containing a backbone modified glutamine
Hing L. Sham William Rosenbrook Warren Kati David A. Betebenner Norman E. Wideburg Ayda Saldivar Jacob J. Plattner and Daniel W. Norbeck
pg 1081; DOI:
10.1039/P19950001081
PDF
The behaviour of the furazan-N-methanide analogue of the furoxan system. Ring expansion: new routes to 6H-1,2,5-oxadiazines. A combined experimental and theoretical study
Richard N. Butler Karen M. Daly John M. McMahon and Luke A. Burke
pg 1083; DOI:
10.1039/P19950001083
PDF
Efficient regiospecific synthesis of two cytotoxic furonaphthoquinones, 5,7-dimethoxy-4,9-dihydronaphtho[2,3-b]furan-4,9-dione and 5,6,7-trimethoxy-4,9-dihydronaphtho[2,3-b]furan-4,9-dione
Philip J. Perry Vasilios H. Pavlidis John A. Hadfield and Ian G. C. Coutts
pg 1085; DOI:
10.1039/P19950001085
PDF
Simple synthetic approach to 6-oxa steroids. Synthesis of 6-oxa-5-pregnane-3,20-dione
Daniel Nicoletti Alberto A. Ghini Adriana L. Brachet-Cota and Gerardo Burton
pg 1089; DOI:
10.1039/P19950001089
PDF
S-Phenylacetamidomethyl (Phacm): an orthogonal cysteine protecting group for Boc and Fmoc solid-phase peptide synthesis strategies
Miriam Royo Jordi Alsina Ernest Giralt Urszula Slomcyznska and Fernando Albericio
pg 1095; DOI:
10.1039/P19950001095
PDF
Synthesis of novel inhibitors of electron transport
G. Stuart Cockerill Philip C. Levett and Donald A. Whiting
pg 1103; DOI:
10.1039/P19950001103
PDF
Synthesis of pyrrolidin-2-ones by 5-endo-trigonal radical cyclisation of N-vinyl-2,2-bis(phenylsulfanyl)acetamides
Tatsunori Sato Noriko Chono Hiroyuki Ishibashi and Masazumi Ikeda
pg 1115; DOI:
10.1039/P19950001115
PDF
Penitremones A–C, Penicillium metabolites containing an oxidised penitrem carbon skeleton giving insight into structure–tremorgenic relationships
Jyotigna T. Naik Peter G. Mantle Richard N. Sheppard and Eric S. Waight
pg 1121; DOI:
10.1039/P19950001121
PDF
Cyclopenta[b]indoles. Part 1. Synthesis of cyclopenta[b]indoles by formal [3 + 2] addition of indolylmethyl cations to alkenes
Carrie-Ann Harrison Ralf Leineweber Christopher J. Moody and Jonathan M. J. Williams
pg 1127; DOI:
10.1039/P19950001127
PDF
Cyclopenta[b]indoles. Part 2. Model studies towards the tremorgenic mycotoxins
Carrie-Ann Harrison P. Mark Jackson Christopher J. Moody and Jonathan M. J. Williams
pg 1131; DOI:
10.1039/P19950001131
PDF
Preparation of oxonanes and azonanes by oxidative ring expansion: synthesis of obtusan
David S. Brown Mark C. Elliott Christopher J. Moody and Timothy J. Mowlem
pg 1137; DOI:
10.1039/P19950001137
PDF
New syntheses of arylphosphinic acids from the reaction of ethyl diethoxymethylphosphinate with aryl bromides and phenols
Stuart N. L. Bennett and Roger G. Hall
pg 1145; DOI:
10.1039/P19950001145
PDF
Hydrocyanation of some ,-unsaturated ketones, and the synthesis of some unusual isoxazoles
Wesley Cocker David H. Grayson and Patrick V. R. Shannon
pg 1153; DOI:
10.1039/P19950001153
PDF
Synthesis of fluorescent derivatives of 3-O-(6-aminohexanoyl)pyrimidine nucleosides 5-triphosphates that act as DNA polymerase substrates reversibly tagged at C-3
Robert S. Sarfati Thomas Berthod Catherine Guerreiro and Bruno Canard
pg 1163; DOI:
10.1039/P19950001163
PDF
Synthesis of the potent influenza neuraminidase inhibitor 4-guanidino Neu5Ac2en. X-Ray molecular structure of 5-acetamido-4-amino-2,6-anhydro-3,4,5-trideoxy-D-erythro-L-gluco-nononic acid
Malcolm Chandler Mark J. Bamford Richard Conroy Brian Lamont Bina Patel Vipulkumar K. Patel Ian P. Steeples Richard Storer Niall G. Weir Michael Wright and Christopher Williamson
pg 1173; DOI:
10.1039/P19950001173
PDF
Synthesis of 6-, 7- and 8-carbon sugar analogues of potent anti-influenza 2,3-didehydro-2,3-dideoxy-N-acetylneuraminic acid derivatives
Mark J. Bamford Julia Castro Pichel Wahid Husman Bina Patel Richard Storer and Niall G. Weir
pg 1181; DOI:
10.1039/P19950001181
PDF
Approaches to carbocyclic analogues of the potent neuraminidase inhibitor 4-guanidino-Neu5Ac2en. X-Ray molecular structure of N-[(1S,2S,6R)-2-azido-6-benzyloxymethyl-4-formylcyclohex-3-enyl]acetamide
Malcolm Chandler Richard Conroy Anthony W. J. Cooper R. Brian Lamont Jan J. Scicinski James E. Smart Richard Storer Niall G. Weir Richard D. Wilson and Paul G. Wyatt
pg 1189; DOI:
10.1039/P19950001189
PDF
Corrigenda
M. Cavazza G. Guella L. Nucci F. Pergola N. Bicchierini F. Pietra Takumi Oshima Kazushi Tamada Toshikazu Nagai Hiroshi Suginome Takahiko Kondoh Camelia Gogonea Vishwakarma Singh Hitoshi Got and Eiji sawa
pg 1199; DOI:
10.1039/P19950001199
PDF
Conference diary

pg viif; DOI:
10.1039/P1995000viif
PDF

Issue 10


Front cover

pg X041; DOI:
10.1039/P199500FX041
PDF
Back cover

pg X043; DOI:
10.1039/P199500BX043
PDF
Contents pages

pg P111; DOI:
10.1039/P199500FP111
PDF
Back matter

pg P119; DOI:
10.1039/P199500BP119
PDF
Conversion of one enantiomer of the carbocyclic nucleoside synthon 2-azabicyclo[2.2.1]hept-5-en-3-one into the other
Christopher F. Palmer and Raymond McCague
pg 1201; DOI:
10.1039/P19950001201
PDF
Synthesis of pyrazole fatty ester derivatives in water: a sonochemical approach
Marcel S. F. Lie Ken Jie and Prabhavathi Kalluri
pg 1205; DOI:
10.1039/P19950001205
PDF
Preparation and reactions of lithium indolyl(dimethyl)zincates
Yoshinori Kondo Nobuo Takazawa Akihiro Yoshida and Takao Sakamoto
pg 1207; DOI:
10.1039/P19950001207
PDF
Synthesis of 3-hydroxythiophenes and thiophen-3(2H)-ones by pyrolysis of alkylsulfanylmethylene Meldrum's acid derivatives
Gordon A. Hunter and Hamish McNab
pg 1209; DOI:
10.1039/P19950001209
PDF
Pigments of fungi. Part 41. Synthesis of (S)-(+)- and ()-dermolactone; stereochemistry of dermolactone from the Australian fungus Dermocybe sanguinea(Wulf. ex Fr.) Wnsche sensu Cleland
Ann S. Cotterill Melvyn Gill and Nives M. Milanovic
pg 1215; DOI:
10.1039/P19950001215
PDF
Some pyrrolopyrimidine chemistry directed to the synthesis of tricyclic purine analogues
David M. Williams and Daniel M. Brown
pg 1225; DOI:
10.1039/P19950001225
PDF
Chemistry of the mycalamides, antiviral and antitumour compounds from a marine sponge. Part 5. Acid-catalysed hydrolysis and acetal exchange, double bond additions and oxidation reactions
Andrew M. Thompson John W. Blunt Murray H. G. Munro and Nigel B. Perry
pg 1233; DOI:
10.1039/P19950001233
PDF
On the reaction between 3-bromo-2-nitrobenzo[b]thiophene and some amines: a novel aromatic nucleophilic substitution with rearrangement
Francesco Guerrera Loredana Salerno Liliana Lamartina and Domenico Spinelli
pg 1243; DOI:
10.1039/P19950001243
PDF
Synthesis of enantiomerically pure (R)- and (S)-2-sulfanylpropanoic acids (thiolactic acid) from ethyl (S)-lactate using pig liver esterase
Robert P. Hof and Richard M. Kellogg
pg 1247; DOI:
10.1039/P19950001247
PDF
Synthesis of all four diastereoisomers of 4-(carboxymethyl)proline, a conformationally constrained analogue of 2-aminoadipic acid
Roberto Pellicciari Loredana Arenare Paolo De Caprariis Benedetto Natalini Maura Marinozzi and Alessandro Galli
pg 1251; DOI:
10.1039/P19950001251
PDF
Dimethyl 3-chloroprop-1-en-2-ylphosphonate. Part 2. Alkylation of amines, phosphines and phosphites
Igor E. Gurevich and John C. Tebby
pg 1259; DOI:
10.1039/P19950001259
PDF
Directed lithiation of unprotected benzoic acids
Bernard Bennetau Jacques Mortier Joël Moyroud and Jean-Luc Guesnet
pg 1265; DOI:
10.1039/P19950001265
PDF
Synthesis of ()-[4a,4b,10b,12a]-9-halogeno-2-methyl-1,2,3,4,4a,4b,5,6,10b,11,12,12a-dodecahydronaphtho[2,1-]isoquinolines
Graham L. Patrick
pg 1273; DOI:
10.1039/P19950001273
PDF
Stereocontrol in cyclisation of dioxolanyl radicals
Andrei S. Batsanov Michael J. Begley Rodney J. Fletcher John A. Murphy and Michael S. Sherburn
pg 1281; DOI:
10.1039/P19950001281
PDF
Biocatalytic preparation of chiral alcohols by enantioselective reduction with immobilized cells of carrot
Yoshihiko Akakabe Mirai Takahashi Makoto Kamezawa Keiichi Kikuchi Hojun Tachibana Takehiko Ohtani and Yoshinobu Naoshima
pg 1295; DOI:
10.1039/P19950001295
PDF
Medium-sized cyclophanes. Part 36. Synthesis and conformational studies of dimethoxy[m.n]metacyclophanes
Takehiko Yamato Jun-ichi Matsumoto Mitsuhiro Sato Kozo Noda and Masashi Tashiro
pg 1299; DOI:
10.1039/P19950001299
PDF
Bromination–dehydrobromination route to some naturally occurring 1,6-dioxaspiro[4.4]-nonenes and -nonadienes
Yong Qiang Tu Karl A. Byriel Colin H. L. Kennard and William Kitching
pg 1309; DOI:
10.1039/P19950001309
PDF
Synthesis of N-aminomethylpyrrolidin-2-ones
Ping Chen Dong-Jin Suh and Michael B. Smith
pg 1317; DOI:
10.1039/P19950001317
PDF
Photochromic heterocyclic fulgides. Part 8. The condensation of 2,6-dichlorobenzaldehyde with diethyl [1-(2,5-dimethyl-3-furyl)ethylidene]succinate to give 6-chloro-2-(2,5-dimethyl-3-furyl)-1H-benzocycloheptene-3,4-dicarboxylic anhydride and photochromic (7S,7aS)-7-(2,6-dichlorophenyl)-2,4,7a-trimethyl-7,7a-dihydrobenzofuran-5,6-dicarboxylic anhydride
Harry G. Heller Christopher J. Morgan and Matthew J. Ottaway
pg 1323; DOI:
10.1039/P19950001323
PDF
Conference diary

pg viig; DOI:
10.1039/P1995000viig
PDF

Issue 11


Front cover

pg X045; DOI:
10.1039/P199500FX045
PDF
Back cover

pg X047; DOI:
10.1039/P199500BX047
PDF
Contents pages

pg P121; DOI:
10.1039/P199500FP121
PDF
Back matter

pg P129; DOI:
10.1039/P199500BP129
PDF
Electrochemical fluorination of 4-trimethylsilylazetidin-2-ones: an efficient and regioselective preparation of 4-fluoroazetidin-2-ones
Kohji Suda Katsumi Hotoda Mitsuaki Aoyagi and Toshikatsu Takanami
pg 1327; DOI:
10.1039/P19950001327
PDF
A direct and stereoselective route to (Z)-2-iodoalk-2-enes via-oxido phosphonium ylides
Yanchang Shen and Shu Gao
pg 1331; DOI:
10.1039/P19950001331
PDF
Phosphoramidate mediated conversion of tricarbonyl(vinylketene)iron(0) complexes into tricarbonyl(vinylketenimine)iron(0) complexes
Stephen A. Benyunes Susan E. Gibson (née Thomas) and James A. Stern
pg 1333; DOI:
10.1039/P19950001333
PDF
Potential mechanism-based tyrosine kinase inhibitors. Part 2. Design and synthesis of peptides containing heterocyclic tyrosine analogues
David M. Andrews Mary Gregoriou Timothy C. M. Page Josephine M. Peach and Andrew J. Pratt
pg 1335; DOI:
10.1039/P19950001335
PDF
The squalestatins: cleavage of the bicyclic core via the novel 6,8-dioxabicyclo[3.2.1]octane ring system
Panayiotis A. Procopiou Esme J. Bailey Chuen Chan Graham G. A. Inglis Michael G. Lester Anton R. P. Srikantha Philip J. Sidebottom and Nigel S. Watson
pg 1341; DOI:
10.1039/P19950001341
PDF
Trapping of translocated radicals by tetrathiafulvalene radical cation
John A. Murphy and Stephen J. Roome
pg 1349; DOI:
10.1039/P19950001349
PDF
SN2 Ring opening of aziridines bearing an ,-unsaturated ester group with organocopper reagents. A new stereoselective synthetic route to (E)-alkene dipeptide isosteres
Nobutaka Fujii Kazuo Nakai Hirokazu Tamamura Akira Otaka Norio Mimura Yoshihisa Miwa Tooru Taga Yoshinori Yamamoto and Toshiro Ibuka
pg 1359; DOI:
10.1039/P19950001359
PDF
Chemoselectivity and stereoselectivity of cyclisation of -diazocarbonyls leading to oxygen and sulfur heterocycles catalysed by chiral rhodium and copper catalysts
Tao Ye Concepción Fernández García and M. Anthony McKervey
pg 1373; DOI:
10.1039/P19950001373
PDF
Reactions of tosyl azide with 2-phenoxy- and 2-phenylsulfanyl-2,3-dihydro-1H-indane-1,3-dione. Unexpected reactivity of intermediate 4-acyl-5-hydroxy-1-tosyltriazolines
Luisa Benati Gianluca Calestani Pier Carlo Montevecchi and Piero Spagnolo
pg 1381; DOI:
10.1039/P19950001381
PDF
Synthesis of 4-thia-2-azapodophyllotoxin, a new analogue of the antitumour lignan podophyllotoxin
Yukio Hitotsuyanagi Masatsugu Kobayashi Koichi Takeya and Hideji Itokawa
pg 1387; DOI:
10.1039/P19950001387
PDF
Approach to the synthesis of 4-demethylforskolin (19-norforskolin)
Jerry J. Harnett James K. Sutherland and Hua Yang
pg 1391; DOI:
10.1039/P19950001391
PDF
The chemoselective cyclisation of unsymmetrical -diketones to cyclopentenones by directed aldol reaction using a magnesium chelate
Michael L. F. Cadman Leslie Crombie Stephen Freeman and Jayshree Mistry
pg 1397; DOI:
10.1039/P19950001397
PDF
Dioxolane nucleosides and their phosphonate derivatives: synthesis and hydrolytic stability
Ekaterina V. Efimtseva Sergey N. Mikhailov Sergey Meshkov Teemu Hankamäki Mikko Oivanen and Harri Lönnberg
pg 1409; DOI:
10.1039/P19950001409
PDF
Synthesis of novel carbo- and heteropolycycles. Part 30. 1,3-Dipolar cycloaddition of nitrile functions with some selected nitrones. Efficient synthesis of 2,3-dihydro-1,2,4-oxadiazole derivatives
Yang Yu Naoto Watanabe Masatomi Ohno and Shoji Eguchi
pg 1417; DOI:
10.1039/P19950001417
PDF
Asymmetric reduction of a carbon–nitrogen double bond: enantioselective synthesis of 4,5-dihydro-3H-2,3-benzodiazepines
István Ling Benjamin Podányi Tamás Hámori and Sándor Sólyom
pg 1423; DOI:
10.1039/P19950001423
PDF
Synthesis of azophenolic crown ethers of Cs symmetry incorporating cis-1-phenylcyclohexane-1,2-diol residues as a steric barrier and diastereotopic face selectivity in complexation of amines by their diastereotopic faces
Koichiro Naemura Sachiko Takeuchi Masaki Asada Koji Ueno Keiji Hirose Yoshito Tobe Takahiro Kaneda and Yoshiteru Sakata
pg 1429; DOI:
10.1039/P19950001429
PDF
Furan-2(3H)- and -2(5H)-ones. Part 6. Di--methane rearrangement of the -substituted 4-benzylfuran-2(5H)-one system
Osamu Muraoka Genzoh Tanabe Mié Higashiura Toshie Minematsu and Takefumi Momose
pg 1437; DOI:
10.1039/P19950001437
PDF
Studies on fused pyrimidine derivatives. Part 14. Formation and transformation of [4 + 2] cycloadducts, cyclohepta[g]quinazoline derivatives, by the reaction of 5-(arylaminomethylene)-1,3-dimethyl-6-methyleneperhydropyrimidine-2,4-diones with tropone
Ken Ikuno Takashi Kobayashi Toshio Harada Michihiko Noguchi and Akikazu Kakehi
pg 1445; DOI:
10.1039/P19950001445
PDF
Studies on fused pyrimidine derivatives. Part 15. Features and mechanistic considerations of the reaction of 5-(alkylaminomethylene)-6-methyleneperhydropyrimidine-2,4-diones with tropone
Takashi Kobayashi Ken Ikuno Michihiko Noguchi and Akikazu Kakehi
pg 1453; DOI:
10.1039/P19950001453
PDF
Photocleavage of the C–O bond of 9-phenanthrylmethyl -anilinoalkyl ethers via photo-induced intramolecular electron transfer
Akira Sugimoto Satoshi Kimoto Tomohiro Adachi and Hiroo Inoue
pg 1459; DOI:
10.1039/P19950001459
PDF
Conference diary

pg viih; DOI:
10.1039/P1995000viih
PDF

Issue 12


Front cover

pg X049; DOI:
10.1039/P199500FX049
PDF
Back cover

pg X051; DOI:
10.1039/P199500BX051
PDF
Contents pages

pg P133; DOI:
10.1039/P199500FP133
PDF
Back matter

pg P143; DOI:
10.1039/P199500BP143
PDF
Enantiocomplementary asymmetric epoxidation of selected enones using poly-L-leucine and poly-D-leucine
M. Elena Lasterra Sánchez and Stanley M. Roberts
pg 1467; DOI:
10.1039/P19950001467
PDF
1,4-Asymmetric induction in reactions between [2-(1-alkoxyalkyl)propenyl](tributyl)stannanes and aldehydes promoted by tin(IV) halides
Michelangelo Gruttadauria and Eric J. Thomas
pg 1469; DOI:
10.1039/P19950001469
PDF
Nucleophilic aromatic substitution of 2-sulfonyl-substituted 1-methoxynaphthalenes with Grignard reagents
Tetsutaro Hattori Mikio Suzuki Yasuko Komuro and Sotaro Miyano
pg 1473; DOI:
10.1039/P19950001473
PDF
Azoles. Part II. Synthesis of imidazole-2(and -5)-carbaldehydes and derivatives of imidazo[1,2-b]isoquinoline; transmetallation of imidazol-5-yllithium compounds
Brian Iddon Anders K. Petersen Jan Becher and Nils J. Christensen
pg 1475; DOI:
10.1039/P19950001475
PDF
Synthesis and biological activity of new C-6 and C-7 substituted vinyloxyimino-penicillins and -cephalosporins
Stephen C. M. Fell Michael J. Pearson George Burton and John S. Elder
pg 1483; DOI:
10.1039/P19950001483
PDF
Synthesis of secasterone and further epimeric 2,3- epoxybrassinosteroids
Brunhilde Voigt Suguru Takatsuto Takao Yokota and Günter Adam
pg 1495; DOI:
10.1039/P19950001495
PDF
Conversion of benzene and chlorobenzene into polyhydroxylated cyclohexane derivatives related to cyclophellitol
Stanley M. Roberts and Peter W. Sutton
pg 1499; DOI:
10.1039/P19950001499
PDF
Enzymatic Baeyer–Villiger oxidations of some bicyclo[2.2.1]heptan-2-ones using monooxygenases from Pseudomonas putida NCIMB 10007: enantioselective preparation of a precursor of azadirachtin
René Gagnon Gideon Grogan Stanley M. Roberts Raffaella Villa and Andrew J. Willetts
pg 1505; DOI:
10.1039/P19950001505
PDF
Synthesis and the absolute configuration of the sesquiterpene aldehyde tridensenal from the Taiwanese liverwort Bazzania tridens
Motoo Tori Naomi Uchida Aya Sumida Hirosuke Furuta and Yoshinori Asakawa
pg 1513; DOI:
10.1039/P19950001513
PDF
1H and 13C NMR characterization of new oleuropein aglycones
Rita Limiroli Roberto Consonni Gianluca Ottolina Vincenzo Marsilio Giorgio Bianchi and Lucia Zetta
pg 1519; DOI:
10.1039/P19950001519
PDF
Synthesis of vinylsilanes by silyl-cupration of acetylenes using tert-butyldiphenylsilyl-cuprate reagents
Asunción Barbero Purificación Cuadrado Ian Fleming Ana M. González Francisco J. Pulido and Alicia Sánchez
pg 1525; DOI:
10.1039/P19950001525
PDF
Reactions of cyclic -keto esters and other enol derivatives with 3-acetoxyamino-2-isopropylquinazolin-4(3H)-one: further oxidation of the cyclic -(3,4-dihydro-2-isopropyl-4-oxoquinazolin-3-yl)amino ketones with lead tetraacetate leading to ring-expansion (in dichloromethane) and ring-cleavage (in methanol)
Robert S. Atkinson Emma Barker Paul J. Edwards and Gordon A. Thomson
pg 1533; DOI:
10.1039/P19950001533
PDF
Total synthesis of 2-deoxy-2-arafluoro-tubercidin, -toyocamycin, -sangivamycin and certain related nucleosides
Birendra K. Bhattacharya T. Sudhakar Rao and Ganapathi R. Revankar
pg 1543; DOI:
10.1039/P19950001543
PDF
Total synthesis of (–)-ovalicin and analogues from L-quebrachitol
Derek H. R. Barton Sophie Bath David C. Billington Stephan D. Gero Béatrice Quiclet-Sire and Mohammad Samadi
pg 1551; DOI:
10.1039/P19950001551
PDF
Stereoselective syntheses of D-ribo- and L-lyxo-phytosphingosine
Yun-Long Li Xiu-Hong Mao and Yu-Lin Wu
pg 1559; DOI:
10.1039/P19950001559
PDF
Biosynthesis of violacein: oxygenation at the 2-position of the indole ring and structures of proviolacein, prodeoxyviolacein and pseudoviolacein, the plausible biosynthetic intermediates of violacein and deoxyviolacein
Tsutomu Hoshino Toru Hayashi and Taro Odajima
pg 1565; DOI:
10.1039/P19950001565
PDF
2-Deoxy-2-trichloroacetamido-D-glucopyranose derivatives in oligosaccharide synthesis: from hyaluronic acid to chondroitin 4-sulfate trisaccharides
Caroline Coutant and Jean-Claude Jacquinet
pg 1573; DOI:
10.1039/P19950001573
PDF
Ring transformation of the adducts of the polar cycloadditions of 2-benzothiopyrylium salts
Hiroshi Shimizu Shojiro Miyazaki Tadashi Kataoka and Mikio Hori
pg 1583; DOI:
10.1039/P19950001583
PDF
Direct visualization of enzyme inhibitors using a portion mixing inhibitor library containing a quenched fluorogenic peptide substrate. Part 1. Inhibitors for subtilisin Carlsberg
Morten Meldal and Ib Svendsen
pg 1591; DOI:
10.1039/P19950001591
PDF
Formation of polycyclic compounds in the photoreactions of 9-(-anilinoalkyl)phenanthrenes
Akira Sugimoto Noriyuki Fukada Tomohiro Adachi and Hiroo Inoue
pg 1597; DOI:
10.1039/P19950001597
PDF
Synthesis of L-threo- and L-erythro-[1-13C, 2,3-2H2]amino acids: novel probes for conformational analysis of peptide side chains
Makoto Oba Ryuichi Ueno Mika Fukuoka (née Yoshida) Masatsune Kainosho and Kozaburo Nishiyama
pg 1603; DOI:
10.1039/P19950001603
PDF
Synthesis and lyotropic phase behaviour of methyl 3,4-di-O-hexyl- and -di-O-octyl--lactoside and partial O-acetylation of methyl 3,4-di-O-octyl--lactoside
Virginie Langlois and J. Michael Williams
pg 1611; DOI:
10.1039/P19950001611
PDF
Synthesis of partial nonpeptidic peptide mimetics as potential neurotensin agonists and antagonists
Alan P. Kozikowski Dharmpal S. Dodd Javid Zaidi Yuan-Ping Pang Bernadette Cusack and Elliott Richelson
pg 1615; DOI:
10.1039/P19950001615
PDF
Synthetic studies on morphine-based analgesics. Intramolecular Diels–Alder approach to 4a-aryldecahydroisoquinolines
Sheetal Handa Keith Jones and Christopher G. Newton
pg 1623; DOI:
10.1039/P19950001623
PDF
Alternative synthesis of 2-arylpropanoic acids from enolate and aryl halides
Carlos G. Ferrayoli Sara M. Palacios and Rubén A. Alonso
pg 1635; DOI:
10.1039/P19950001635
PDF
Conference diary

pg ixa; DOI:
10.1039/P19950000ixa
PDF

Issue 13


Front cover

pg X053; DOI:
10.1039/P199500FX053
PDF
Back cover

pg X055; DOI:
10.1039/P199500BX055
PDF
Contents pages

pg P145; DOI:
10.1039/P199500FP145
PDF
Back matter

pg P153; DOI:
10.1039/P199500BP153
PDF
A new approach to the synthesis of dipeptides with unnatural amino acids using organozinc chemistry
Michael J. Dunn Sylvie Gomez and Richard F. W. Jackson
pg 1639; DOI:
10.1039/P19950001639
PDF
Oxidation of methyl p-tolyl sulfide with bakers' yeast: preparation of a synthon of the mevinic acid-type hypocholestemic agents
Jean Beecher Ian Brackenridge Stanley M. Roberts Jenny Tang and Andrew J. Willetts
pg 1641; DOI:
10.1039/P19950001641
PDF
Lipase-promoted asymmetric transesterification of 4-alkyloxetan-2-ones with ring-opening
Yota Koichi Kaoru Suginaka and Yukio Yamamoto
pg 1645; DOI:
10.1039/P19950001645
PDF
Ring expansion reactions of isoquinoline derivatives to 2-benzazocine and 3-benzazecine derivatives
Mostafa M. M. Bamatraf John M. Vernon and Giles D. Wilson
pg 1647; DOI:
10.1039/P19950001647
PDF
A phenanthrolinoquinomethane: synthesis and study of precursors
Noemie Fixler Hervé Salez Martine Demeunynck and Jean Lhomme
pg 1649; DOI:
10.1039/P19950001649
PDF
Reactions of N-sulfinylarylamines with 1,4-benzoquinone and 1,4-naphthoquinone: synthesis of N-aryl sulfinamoyl quinones and their hydrolysis to hydroxyquinones
Ananda S. Amarasekara and W. Wimal Pathmasiri
pg 1653; DOI:
10.1039/P19950001653
PDF
Some chemistry of 4,5-dichloro-1,2,3-dithiazolium chloride and its derivatives
Thierry Besson and Charles W. Rees
pg 1659; DOI:
10.1039/P19950001659
PDF
Biosynthesis of aspinonene, a branched pentaketide produced by Aspergillus ochraceus, related to aspyrone
Jens Fuchser Ralf Thiericke and Axel Zeeck
pg 1663; DOI:
10.1039/P19950001663
PDF
Synthesis and use of (E)-1-ethoxy-3-fluoroalkyl-3-hydroxy-4-(4-methylphenylsulfinyl)but-1-enes
Pierfrancesco Bravo Luca Bruché Alessandra Farina Igor I. Gerus Maria T. Kolytcheva Valery P. Kukhar Stefano Valdo Meille and Fiorenza Viani
pg 1667; DOI:
10.1039/P19950001667
PDF
Parasite glycoconjugates. Part 3. Synthesis of substrate analogues of early intermediates in the biosynthetic pathway of glycosylphosphatidylinositol membrane anchors
Sylvain Cottaz John S. Brimacombe and Michael A. J. Ferguson
pg 1673; DOI:
10.1039/P19950001673
PDF
Organolead-mediated arylation of allyl -keto esters: selective synthesis of 2-hydroxyisoflavones
Dervilla M. X. Donnelly Jean-Pierre Finet and Bernard A. Rattigan
pg 1679; DOI:
10.1039/P19950001679
PDF
Synthesis of S-alkyl esters of protected 2-deoxyribonucleoside 3-phosphorothioates. Building blocks for the large-scale synthesis of phosphorothioate analogues of oligodeoxyribonucleotides by the phosphotriester approach in solution
Xiaohai Liu and Colin B. Reese
pg 1685; DOI:
10.1039/P19950001685
PDF
Preparation of optically active derivatives of (1,4/2,3,5)- and (1,2,3,4,5/0)-5-aminocyclopentane-1,2,3,4-tetraols: synthesis of mannostatin A and its enantiomer
Seiichiro Ogawa Hiroshi Kimura Chikara Uchida and Takashi Ohashi
pg 1695; DOI:
10.1039/P19950001695
PDF
Synthesis of trehazolin analogues containing modified sugar moieties
Chikara Uchida Hideo Kitahashi Shinsuke Watanabe and Seiichiro Ogawa
pg 1707; DOI:
10.1039/P19950001707
PDF
New synthesis of hypervalent T-shaped coordination compounds of selenium by the reaction of bis(2-bromoethyl)selenium dibromide with pyridine and its derivatives
Masatsugu Miura Yoshinori Takanohashi Yoichi Habata and Sadatoshi Akabori
pg 1719; DOI:
10.1039/P19950001719
PDF
Cuprous bromide-promoted cyclization of ketene N,S-acetals with prop-2-ynyl bromide: synthesis of regiospecifically substituted and annelated 3-acyl(or nitro)-5-methyl pyrroles
Akhilesh K. Gupta Kethiri R. Reddy Hiriyakkanavar Ila and Hiriyakkanavar Junjappa
pg 1725; DOI:
10.1039/P19950001725
PDF
Addition–cyclization of a diallylmalonic acid ester and related compounds with per(poly)fluoroalkyl iodides using a trichlorolanthanide [LnCl3(cat.)]/Zn system
Wei-Yuan Huang Gang Zhao and Yu Ding
pg 1729; DOI:
10.1039/P19950001729
PDF
Strong inhibitory effect of sugarbiphenylylboronic acid complexes on the hydrolytic activity of -chymotrypsin
Hikaru Suenaga Masafumi Mikami Hiromasa Yamamoto Takaaki Harada and Seiji Shinkai
pg 1733; DOI:
10.1039/P19950001733
PDF
Synthesis of major histocompatibility complex class I binding glycopeptides
Gemma Arsequell John S. Haurum Tim Elliott Raymond A. Dwek and Annemarie C. Lellouch
pg 1739; DOI:
10.1039/P19950001739
PDF
Synthesis of tetrazoles bearing a sugar moiety (sugar tetrazoles). X-Ray molecular structure of (7R,8R,9S,10R)-8,9,10-tribenzyloxy-7-benzyloxymethyl-6-oxa-1,5-pentamethylenetetrazole
Masataka Yokoyama Sachiko Hirano Michio Matsushita Takeshi Hachiya Naoki Kobayashi Misao Kubo Hideo Togo and Hiroko Seki
pg 1747; DOI:
10.1039/P19950001747
PDF
New digitalis steroids. Synthesis of 17-amino 5,14-steroids by thermolysis of 17-azidocarbonyloxymethyl derivatives
Giorgio Fedrizzi Luigi Bernardi Giuseppe Marazzi Piero Melloni and Marco Frigerio
pg 1755; DOI:
10.1039/P19950001755
PDF
Diels–Alder reaction of benzylidene(cyano)methyl-1,3-benzoxa/thiazoles as stable 1-azabuta-1,3-dienes
Masanori Sakamoto Asae Nozaka Mino Shimamoto Hideki Ozaki Yoko Suzuki Sanae Yoshioka Mayumi Nagano Kimio Okamura Tadamasa Date and Osamu Tamura
pg 1759; DOI:
10.1039/P19950001759
PDF
Synthesis of ,-disubstituted acetic acids using low-valent titanium
Mariano García Carmen del Campo Emilio F. Llama and José V. Sinisterra
pg 1771; DOI:
10.1039/P19950001771
PDF
3,4-Di-O-methylcedrusin: synthesis, resolution and absolute configuration
Guy Lemière Mei Gao Alex De Groot Roger Dommisse Josef Lepoivre Luc Pieters and Volker Buss
pg 1775; DOI:
10.1039/P19950001775
PDF
Corrigendum
Jim-Min Fang Chun-Hung Lin Curt W. Bradshaw and Chi-Huey Wong
pg 1781; DOI:
10.1039/P19950001781
PDF
Conference diary

pg viii; DOI:
10.1039/P1995000viii
PDF

Issue 14


Front cover

pg X057; DOI:
10.1039/P199500FX057
PDF
Back cover

pg X059; DOI:
10.1039/P199500BX059
PDF
Contents pages

pg P155; DOI:
10.1039/P199500FP155
PDF
Back matter

pg P163; DOI:
10.1039/P199500BP163
PDF
Synthesis of the 1,4-diazepan-2-one moiety of liposidomycins
Kwan Soo Kim In Haeng Cho Yeong Hee Ahn and Jong Il Park
pg 1783; DOI:
10.1039/P19950001783
PDF
Synthesis and X-ray crystal structure of 1,3,5-tris(fluoren-9-ylidenemethyl)benzene: towards a C48-fragment of [60]-fullerene
Goverdhan Mehta K. Venkateswara Rao and K. Ravikumar
pg 1787; DOI:
10.1039/P19950001787
PDF
The inverse electron-demand Diels–Alder reaction in polymer synthesis. Part 2. Some bis(1,2,4-triazines) as potential bis-diene monomers
Michael J. Bruce Gillian A. McLean Brodyck J. L. Royles David M. Smith and Paul N. Standring
pg 1789; DOI:
10.1039/P19950001789
PDF
Anthraquinone-photocatalysed addition of amines to ,-unsaturated esters: a novel route to indolizidone, pyrrolizidone and related ring systems
Suresh Das J. S. Dileep Kumar K. Shivaramayya and M. V. George
pg 1797; DOI:
10.1039/P19950001797
PDF
Synthesis of bridged azabicyclic compounds using radical translocation reactions of 1-(o-bromobenzoyl)-2-(prop-2-enyl)pyrrolidines
Tatsunori Sato Yasuhiro Kugo Erina Nakaumi Hiroyuki Ishibashi and Masazumi Ikeda
pg 1801; DOI:
10.1039/P19950001801
PDF
Docetaxel (taxotere) derivatives: novel NbCl3-based stereoselective approach to 2-methyldocetaxel
Jean-Noël Denis Abdellatif Fkyerat Yves Gimbert Claire Coutterez Pierre Mantellier Sylvie Jost and Andrew E. Greene
pg 1811; DOI:
10.1039/P19950001811
PDF
Synthesis and characterisation of some novel phthalocyanines containing both oligo(ethyleneoxy) and alkyl or alkoxy side-chains: novel unsymmetrical discotic mesogens
Guy J. Clarkson Neil B. McKeown and Kevin E. Treacher
pg 1817; DOI:
10.1039/P19950001817
PDF
The mechanism of directed remote asymmetric reduction of carbonyl groups via homochiral boronate esters
Gráinne Conole Richard J. Mears Harshani De Silva and Andrew Whiting
pg 1825; DOI:
10.1039/P19950001825
PDF
Alkylation of 6-N-acylated adenosine derivatives by the use of phase transfer catalysis
Keiichi Aritomo Takeshi Wada and Mitsuo Sekine
pg 1837; DOI:
10.1039/P19950001837
PDF
Titanium(IV) mediated reductive aminations of 1-adamantyl methyl ketone: facile preparation of potential antiviral agents rimantadine and its analogues
Sukanta Bhattacharyya
pg 1845; DOI:
10.1039/P19950001845
PDF
Antibiotic peptides from Trichoderma harzianum: harzianins HC, proline-rich 14-residue peptaibols
Sylvie Rebuffat Christophe Goulard and Bernard Bodo
pg 1849; DOI:
10.1039/P19950001849
PDF
Intramolecular 1,3-dipolar cycloaddition at the periphery of heterocyclic systems. Part 1. Facile oxime–nitrone isomerisation at the periphery of pyran and 1-benzopyran
Mitsuhiro Gotoh Takahiro Mizui Bin Sun Ken Hirayama and Michihiko Noguchi
pg 1857; DOI:
10.1039/P19950001857
PDF
Asymmetric Diels–Alder reactions between chiral sugar nitroalkenes and 1-O-substituted buta-1,3-dienes. Synthesis and reactivity of new cyclohexenyl derivatives
José A. Serrano Luis E. Cáceres and Emilio Román
pg 1863; DOI:
10.1039/P19950001863
PDF
Synthesis, resolution and absolute configuration determination of (S)- and (R)-4-formyl-5-hydroxy [2.2]paracyclophane and its application in the asymmetric synthesis of -amino acids
Dmitri Yu. Antonov Yuri N. Belokon Nikolai S. Ikonnikov Svetlana A. Orlova Aleksander P. Pisarevsky Nikolai I. Raevski Valeria I. Rozenberg Elena V. Sergeeva Yuri T. Struchkov Vitali I. Tararov and Evgeni V. Vorontsov
pg 1873; DOI:
10.1039/P19950001873
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Conference diary

pg viij; DOI:
10.1039/P1995000viij
PDF

Issue 15


Front cover

pg X061; DOI:
10.1039/P199500FX061
PDF
Back cover

pg X063; DOI:
10.1039/P199500BX063
PDF
Contents pages

pg P165; DOI:
10.1039/P199500FP165
PDF
Back matter

pg P173; DOI:
10.1039/P199500BP173
PDF
Cerium(IV) ammonium nitrate mediated addition of dimethyl malonate to styrene: a remarkable reaction
Vijay Nair and Jessy Mathew
pg 1881; DOI:
10.1039/P19950001881
PDF
Design and synthesis of a C4-symmetrical hard–soft ditopic metal receptor by calixarene–porphyrin coupling
Takeshi Nagasaki Hiroyuki Fujishima Masayuki Takeuchi and Seiji Shinkai
pg 1883; DOI:
10.1039/P19950001883
PDF
Selective mono-benzylation of methylene active compounds with dibenzyl carbonate: benzylation of phenol
Maurizio Selva Carlos Alberto Marques and Pietro Tundo
pg 1889; DOI:
10.1039/P19950001889
PDF
Carotenoids and related polyenes. Part 3. First total synthesis of fucoxanthin and halocynthiaxanthin using oxo-metallic catalyst
Yumiko Yamano Chisato Tode and Masayoshi Ito
pg 1895; DOI:
10.1039/P19950001895
PDF
Synthesis of DL-threo-3-(1-fluoro-1-methylethyl)- and DL-threo-3-(1,1-difluoroethyl)malic acids. Mechanistic studies of 3-isopropylmalate dehydrogenase
Tetsuya Aoyama Tadashi Eguchi Tairo Oshima and Katsumi Kakinuma
pg 1905; DOI:
10.1039/P19950001905
PDF
Control over absolute (R,S), relative (syn,anti) and geometrical (E,Z) stereochemistry in the synthesis of allylically substituted alkenes from diphenylphosphinoyl epoxy alcohols
Jonathan Clayden Andrew B. McElroy and Stuart Warren
pg 1913; DOI:
10.1039/P19950001913
PDF
Biosynthesis of (+)-cubenene and (+)-epicubenol by cell-free extracts of cultured cells of Heteroscyphus planus and cyclization of [2H]farnesyl diphosphates
Kensuke Nabeta Kazuyoshi Kigure Masaru Fujita Tomomi Nagoya Takehiro Ishikawa Hiroshi Okuyama and Toshihide Takasawa
pg 1935; DOI:
10.1039/P19950001935
PDF
Radical substitution on a thioester by a methyl radical generated from methyl(L)cobaloxime
Masaru Tada Takao Yoshihara and Kiyohiko Sugano
pg 1941; DOI:
10.1039/P19950001941
PDF
Synthesis of chiral diazanedicarboxylate and diazenedicarboxylate esters: electrophilic amination reactions of achiral ester and amide enolates
Joanna M. Harris Evon A. Bolessa Aubrey J. Mendonca Sheng-Chu Feng and John C. Vederas
pg 1945; DOI:
10.1039/P19950001945
PDF
Synthesis of macrocyclic diazanedicarboxylate and diazenedicarboxylate esters containing a steroid skeleton: an unusual oxidation of bromide to bromine by a strained diazenedicarboxylate ester. X-Ray molecular structure of 3-(3-hydroxypropyl)-24-nor-5-cholan-7-ol diazane-1,2-dicarboxylate cyclic diester
Joanna M. Harris Evon A. Bolessa and John C. Vederas
pg 1951; DOI:
10.1039/P19950001951
PDF
Electro-organic reactions. Part 42. The diastereoselective cathodic hydrodimerisation of cinnamate esters; preparative aspects
James H. P. Utley Mustafa Güllü and Majid Motevalli
pg 1961; DOI:
10.1039/P19950001961
PDF
New synthesis of carboxin and oxycarboxin pesticides: application to the preparation of their new analogues substituted at the C-2 methyl group
Romualdo Caputo Carla Ferreri Annalisa Guaragna Giovanni Palumbo and Silvana Pedatella
pg 1971; DOI:
10.1039/P19950001971
PDF
Corrigenda
Mark J. Bamford Julia Castro Pichel Wahid Husman Bina Patel Richard Storer Niall G. Weir John A. Murphy and Stephen J. Romme
pg 1975; DOI:
10.1039/P19950001975
PDF
Conference diary

pg viik; DOI:
10.1039/P1995000viik
PDF

Issue 16


Front cover

pg X065; DOI:
10.1039/P199500FX065
PDF
Back cover

pg X067; DOI:
10.1039/P199500BX067
PDF
Contents pages

pg P177; DOI:
10.1039/P199500FP177
PDF
Back matter

pg P185; DOI:
10.1039/P199500BP185
PDF
Parasite glycoconjugates. Part 4. Chemical synthesis of disaccharide and phosphorylated oligosaccharide fragments of Leishmania donovani antigenic lipophosphoglycan
Andrey V. Nikolaev Trevor J. Rutherford Michael A. J. Ferguson and John S. Brimacombe
pg 1977; DOI:
10.1039/P19950001977
PDF
Tripolar mesoionic compounds
Shuki Araki Jiro Mizuya Naomitsu Aoyama and Yasuo Butsugan
pg 1989; DOI:
10.1039/P19950001989
PDF
Synthesis of photoactivatable fluorescein derivatives bearing side chains with varying properties
John E. T. Corrie and David R. Trentham
pg 1993; DOI:
10.1039/P19950001993
PDF
Synthesis of phosphorothioate esters of L-phenyl-lactic acid as transition-state inhibitors of carboxypeptidase A
Jacqueline M. Hill and Gordon Lowe
pg 2001; DOI:
10.1039/P19950002001
PDF
Regio- and enantio-selective catalytic epoxidation of conjugated dienes
Kaare G. Rasmussen Dorte S. Thomsen and Karl Anker Jørgensen
pg 2009; DOI:
10.1039/P19950002009
PDF
Improved preparation of -amyloid(1–43): structural insight leading to optimised positioning of N-(2-hydroxy-4-methoxybenzyl)(Hmb) backbone amide protection
Martin Quibell William G. Turnell and Tony Johnson
pg 2019; DOI:
10.1039/P19950002019
PDF
Synthesis and cathodic cleavage of a set of substituted benzenesulfonamides including the corresponding tert-butyl sulfonylcarbamates: pKa of sulfonamides
Barthélémy Nyasse Leif Grehn Ulf Ragnarsson Hernani L. S. Maia Luis S. Monteiro Ivo Leito Ilmar Koppel and Juta Koppel
pg 2025; DOI:
10.1039/P19950002025
PDF
Isomerisation of 4-aryl-4-methylhex-5-en-2-ones to 5-aryl-4-methylhex-5-en-2-ones by an intramolecular ene-retro ene reaction sequence
A. Srikrishna K. Krishnan S. Venkateswarlu and P. Praveen Kumar
pg 2033; DOI:
10.1039/P19950002033
PDF
Chemistry of silyl thioketones. Part 8. Photo-induced cycloadditions of silyl thioketones with olefins
Bianca Flavia Bonini Mauro Comes Franchini Mariafrancesca Fochi Germana Mazzanti Alfredo Ricci Paolo Zani and Binne Zwanenburg
pg 2039; DOI:
10.1039/P19950002039
PDF
Preparation of alkyl- and aryl-amino[2H2]methylphosphinic acids
Sylvie Berté-Verrando François Nief Carl Patois and Philippe Savignac
pg 2045; DOI:
10.1039/P19950002045
PDF
Asymmetric synthesis of steroidal Trger's base analogues. X-Ray molecular structure of methyl 3,12-{6H,12H-5,11-methanodibenzo[b,f][1,5]diazocine-2,8-bisacetoxy}-5-cholan-24-oate
Uday Maitra Braja Gopal Bag Photon Rao and Douglas Powell
pg 2049; DOI:
10.1039/P19950002049
PDF
Model for the functional active site of Baeyer–Villigerases. X-Ray crystal data for (1S,2R,5R,8S,1R)-8-endo-benzoyloxy-N-(1-phenylethyl)bicyclo[3.3.0]octane-2-endo-carboxamide
David R. Kelly Christopher J. Knowles Jassem G. Mahdi Michael A. Wright Ian N. Taylor David E. Hibbs Michael B. Hursthouse Adel K. Mish'al Stanley M. Roberts Peter W. H. Wan Gideon Grogan and Andrew J. Willetts
pg 2057; DOI:
10.1039/P19950002057
PDF
Metabolites of the higher fungi. Part 28. Globoscinic acid and globoscin, a labile acid–lactone system from Xylaria globosa and Xylaria obovata
Monilola Adeboya Raymond L. Edwards Thomas Laessøe Derek J. Maitland and Anthony S. J. Whalley
pg 2067; DOI:
10.1039/P19950002067
PDF
Conference diary

pg viil; DOI:
10.1039/P1995000viil
PDF

Issue 17


Front cover

pg X069; DOI:
10.1039/P199500FX069
PDF
Back cover

pg X071; DOI:
10.1039/P199500BX071
PDF
Contents pages

pg P187; DOI:
10.1039/P199500FP187
PDF
Regioselectivity in the nickel-catalysed coupling of cyclic carbonates of but-3-ene-1,2-diols with organoborates
Ryo Mizojiri and Yuichi Kobayashi
pg 2073; DOI:
10.1039/P19950002073
PDF
Synthesis and reactivity of tricarbonyl(indan-2-one)chromium(0)
E. Lucy M. Cowton Susan E. Gibson (née Thomas) Michael J. Schneider and Mark H. Smith
pg 2077; DOI:
10.1039/P19950002077
PDF
Ring-opening desulfurization of 1,2,3-thiadiazolium salts with N-nucleophiles
Gerrit L'abbé Peggy Vossen Wim Dehaen and Suzanne Toppet
pg 2079; DOI:
10.1039/P19950002079
PDF
Keynote article. Nickel catalysed coupling of allylamines and boronic acids
Barry M. Trost and Michel D. Spagnol
pg 2083; DOI:
10.1039/P19950002083
PDF
1,2,3-Dithiazoles and new routes to 3,1-benzoxazin-4-ones, 3,1-benzothiazin-4-ones and N-arylcyanothioformamides
Thierry Besson Kumaraswamy Emayan and Charles W. Rees
pg 2097; DOI:
10.1039/P19950002097
PDF
2-Alkoxy-3-oxoalkyl-tetrahydropyrans and -tetrahydrofurans: versatile intermediates in heterocyclic synthesis
Pierre Duhamel Abdallah Deyine Gilles Dujardin Gérard Plé and Jean-Marie Poirier
pg 2103; DOI:
10.1039/P19950002103
PDF
Two alternative conformational states of ,-dialkylglycyl-L-prolyl sequences governed by presence/absence of an NH group directly following the proline residue. X-Ray crystal and molecular structures of Boc-D-Iva-L-Pro-NHBzl and Boc-L-Iva-L-Pro-NHBzl
Masao Kawai Yoshimasa Omori Hatsuo Yamamura Yasuo Butsugan Tooru Taga and Yoshihisa Miwa
pg 2115; DOI:
10.1039/P19950002115
PDF
Preparation of -methoxyallylphosphonates and their conversion into 2-methoxyalka-1,3-dienes
Kevin Fettes Leslie McQuire and Alistair W. Murray
pg 2123; DOI:
10.1039/P19950002123
PDF
A potential photoaffinity probe for labelling the active site of aequorin: a photolabile coelenterazine analogue with a trifluoromethyldiazirine group
Feng Qi Chen Jing Ling Zheng Takashi Hirano Haruki Niwa Yoshihiro Ohmiya and Mamoru Ohashi
pg 2129; DOI:
10.1039/P19950002129
PDF
Reactivity of [bis(1-adamantylcarbonyloxy)iodo]arenes in substitution and addition reactions
Hideo Togo Rie Taguchi Kentaro Yamaguchi and Masataka Yokoyama
pg 2135; DOI:
10.1039/P19950002135
PDF
Synthesis and thermal decomposition of azidovinylbenzo[b]thiophenes
Alessandro Degl'Innocenti Maria Funicello Patrizia Scafato Piero Spagnolo and Paolo Zanirato
pg 2141; DOI:
10.1039/P19950002141
PDF
Synthesis and oxidation of the decarbonylated adducts generated from alkenes and tricarbonyl(vinylketene)iron(0) complexes
Susan E. Gibson (née Thomas) Stephen P. Saberi Alexandra M. Z. Slawin Paul D. Stanley Mark F. Ward David J. Williams and Paul Worthington
pg 2147; DOI:
10.1039/P19950002147
PDF
Carbon–carbon bond formation and reduction of aldehydes, ketones and acetals with silylated nucleophiles catalysed by tetracyanoethylene
Tsuyoshi Miura and Yukio Masaki
pg 2155; DOI:
10.1039/P19950002155
PDF
Formal total syntheses of (–)-oudemansins A, B and X based on a lipase-catalysed hydrolysis of an acetate
Hiroyuki Akita Cheng Yu Chen and Shinji Nagumo
pg 2159; DOI:
10.1039/P19950002159
PDF
Comparison of N-Dts and N-Aloc in the solid-phase syntheses of O-GlcNAc glycopeptide fragments of RNA-polymerase II and mammalian neurofilaments
Ernst Meinjohanns Antonio Vargas-Berenguel Morten Meldal Hans Paulsen and Klaus Bock
pg 2165; DOI:
10.1039/P19950002165
PDF
Selective synthesis of unsymmetrical 2,2-dihydroxylated biaryls via electrophilic arylation of metal phenolates with p-benzoquinone monoketals
Giovanni Sartori Raimondo Maggi Franca Bigi Simone Giacomelli Cecilia Porta Attilio Arienti and Gabriele Bocelli
pg 2177; DOI:
10.1039/P19950002177
PDF
Facial selectivity in the hydroboration of androst-4-enes
James R. Hanson Peter B. Hitchcock Mansur D. Liman and Sivajini Nagaratnam
pg 2183; DOI:
10.1039/P19950002183
PDF
4-Hydroxymethyl steroids related to aphidicolin
Juliette A. Boynton and James R. Hanson
pg 2189; DOI:
10.1039/P19950002189
PDF
Synthesis of the glycidol (1R,2R)-1-iodo-2-(triphenylsilyloxy)cyclopropane: new rearrangements of 2,3-epoxy-3-(trialkyl/arylsilyl)-propan-1-ols
Barbara Achmatowicz Piotr Raubo and Jerzy Wicha
pg 2193; DOI:
10.1039/P19950002193
PDF
Corrigenda
Marcel S. F. Lie Ken Jie Prabhavathi Kalluri Yang Yu Naoto Watanabe Masatomi Ohno and Shoji Eguchi
pg 2197; DOI:
10.1039/P19950002197
PDF
Conference diary

pg viim; DOI:
10.1039/P1995000viim
PDF

Issue 18


Front cover

pg X073; DOI:
10.1039/P199500FX073
PDF
Back cover

pg X075; DOI:
10.1039/P199500BX075
PDF
Contents pages

pg P195; DOI:
10.1039/P199500FP195
PDF
Back matter

pg P205; DOI:
10.1039/P199500BP205
PDF
Stereospecific and regiospecific ring opening of glycidol with primary and secondary alcohols mediated by diisobutylaluminium hydride
Ravi Kumar Erukulla Hoe-Sup Byun David C. Locke and Robert Bittman
pg 2199; DOI:
10.1039/P19950002199
PDF
Effective, direct biomimetic synthesis of dibenzocyclooctene lignans by hypervalent iodine oxidation of phenolic dibenzylbutyrolactones
Andrew Pelter Peter Satchwell Robert S. Ward and Keith Blake
pg 2201; DOI:
10.1039/P19950002201
PDF
Enzymatic esterification and de-esterification of carbohydrates: synthesis of a naturally occurring rhamnopyranoside of p-hydroxybenzaldehyde and a systematic investigation of lipase-catalysed acylation of selected arylpyranosides
Nazir B. Bashir Sara J. Phythian Andrew J. Reason and Stanley M. Roberts
pg 2203; DOI:
10.1039/P19950002203
PDF
Enzyme mimics based on cyclic porphyrin oligomers: strategy, design and exploratory synthesis
Harry L. Anderson and Jeremy K. M. Sanders
pg 2223; DOI:
10.1039/P19950002223
PDF
Ligand binding by butadiyne-linked porphyrin dimers, trimers and tetramers
Harry L. Anderson Sally Anderson and Jeremy K. M. Sanders
pg 2231; DOI:
10.1039/P19950002231
PDF
Template-directed synthesis of linear and cyclic butadiyne-linked porphyrin oligomers up to a linear octamer
Sally Anderson Harry L. Anderson and Jeremy K. M. Sanders
pg 2247; DOI:
10.1039/P19950002247
PDF
The roles of templates in the syntheses of porphyrin oligomers
Sally Anderson Harry L. Anderson and Jeremy K. M. Sanders
pg 2255; DOI:
10.1039/P19950002255
PDF
A platinum-linked porphyrin trimer and a complementary aluminium tris[3-(4-pyridyl)acetylacetonate] guest
Lindsey G. Mackay Harry L. Anderson and Jeremy K. M. Sanders
pg 2269; DOI:
10.1039/P19950002269
PDF
Octatetrayne-linked porphyrins: stretched cyclic dimers and trimers with very spacious cavities
Harry L. Anderson Christopher J. Walter Anton Vidal-Ferran Robert A. Hay Philip A. Lowden and Jeremy K. M. Sanders
pg 2275; DOI:
10.1039/P19950002275
PDF
Synthesis of 9-[cis-3-(hydroxymethyl)cyclobutyl]-adenine and -guanine
Vijay Kaiwar Colin B. Reese Emily J. Gray and Stephen Neidle
pg 2281; DOI:
10.1039/P19950002281
PDF
Generation of trimethylsulfonium cation from dimethyl sulfoxide and dimethyl sulfate: implications for the synthesis of epoxides from aldehydes and ketones
Julie Forrester Ray V. H. Jones Peter N. Preston and Elizabeth S. C. Simpson
pg 2289; DOI:
10.1039/P19950002289
PDF
Heterodiene cycloadditions of C2 symmetric 4,5-disubstituted ketene acetals: the nett asymmetric conjugate addition of recyclable acetic ester enolate equivalents to an activated enone
Timothy W. Wallace Ian Wardell Ke-Dong Li Peter Leeming Alan D. Redhouse and S. Richard Challand
pg 2293; DOI:
10.1039/P19950002293
PDF
Amino acids and peptides. Part 42. Application of the 2-adamantyloxycarbonyl (2-Adoc) group to the protection of the imidazole function of histidine in peptide synthesis
Yasuhiro Nishiyama Noriyuki Shintomi Yukihiro Kendo Takako Izumi and Yoshio Okada
pg 2309; DOI:
10.1039/P19950002309
PDF
Iron(III) mediated transformations of cyclopropyltrimethylsilyl ethers. Part 1. Free radical tandem ring expansion–cyclisation reactions for the rapid construction of [n.3.0] bicyclic ring systems
Kevin I. Booker-Milburn and David F. Thompson
pg 2315; DOI:
10.1039/P19950002315
PDF
Synthesis of 3-alkylpyridines. Part 2. Synthesis of both enantiomers of niphatesine C2
Franz Bracher and Thomas Papke
pg 2323; DOI:
10.1039/P19950002323
PDF
Cyclic peptides from higher plants. Part 21. Thionation of the antitumour cyclic pentapeptides, astins A, B and C, from Aster tataricus
Hiroshi Morita Shinji Nagashima Koichi Takeya and Hideji Itokawa
pg 2327; DOI:
10.1039/P19950002327
PDF
Reaction of ortho-lithiated protected anilines with o-hydroxycarbonyl compounds: formation of quino- and pyranoquino-acridines
Catherine Jolivet Christian Rivalle Christiane Huel and Emile Bisagni
pg 2333; DOI:
10.1039/P19950002333
PDF
Chiral crown ethers incorporating D-glucose
Puthuparampil P. Kanakamma Neelakandha S. Mani Uday Maitra and Vijay Nair
pg 2339; DOI:
10.1039/P19950002339
PDF
Fumiquinazolines A–G, novel metabolites of a fungus separated from a Pseudolabrus marine fish
Chika Takahashi Tomochika Matsushita Mitsunobu Doi Katsuhiko Minoura Tetsuro Shingu Yuko Kumeda and Atsushi Numata
pg 2345; DOI:
10.1039/P19950002345
PDF
Total synthesis of balanol: a potent protein kinase C inhibitor of fungal origin
C. P. Adams S. M. Fairway C. J. Hardy D. E. Hibbs M. B. Hursthouse A. D. Morley B. W. Sharp N. Vicker and I. Warner
pg 2355; DOI:
10.1039/P19950002355
PDF
Heterocyclic transformations. Part 7. Unprecedented transformations of 1,3-dialkyl-5-formyluracils to 1,3-dialkyl-7-hydroxyquinazolines
Harjit Singh Palwinder Singh Swapandeep Singh Chimni and Subodh Kumar
pg 2363; DOI:
10.1039/P19950002363
PDF
Conference diary

pg ixb; DOI:
10.1039/P19950000ixb
PDF

Issue 19


Front cover

pg X077; DOI:
10.1039/P199500FX077
PDF
Back cover

pg X079; DOI:
10.1039/P199500BX079
PDF
Contents pages

pg P207; DOI:
10.1039/P199500FP207
PDF
Back matter

pg P217; DOI:
10.1039/P199500BP217
PDF
Acylnitrilium ion initiated spiroannulations in heterocycle synthesis: an application directed toward the total synthesis of the Lycopodium alkaloid ()-serratine
Gregory Luedtke and Tom Livinghouse
pg 2369; DOI:
10.1039/P19950002369
PDF
On the scope of acylnitrilium ion initiated heteroannulations: monocyclizations terminated by unactivated alkenes
David J. Hughes and Tom Livinghouse
pg 2373; DOI:
10.1039/P19950002373
PDF
Se-Demethylation from 8-dimethylamino-1-methylselanylnaphthalene and its Se-oxide: an X-ray structure of a stable selenenic anhydride with a 8-dimethylamino-1-naphthyl ligand: peri Se N interaction
Hisashi Fujihara Hitomi Tanaka and Naomichi Furukawa
pg 2375; DOI:
10.1039/P19950002375
PDF
Unusual behaviour of 4,5-dichloro-1,2,3-dithiazolium chloride (Appel's salt) with 5-aminopyrazoles: a synthetic method of 1H-pyrazolo[3,4-d]thiazoles
Gerrit L'abbé Bart D'hooge and Wim Dehaen
pg 2379; DOI:
10.1039/P19950002379
PDF
New synthesis of unsymmetrical dithia compounds
Keith Smith and Michael Tzimas
pg 2381; DOI:
10.1039/P19950002381
PDF
Uncatalysed trimethylsilyl cyanide addition to aldehydes
Kavita Manju and Sanjay Trehan
pg 2383; DOI:
10.1039/P19950002383
PDF
Pyrylium salts in polyene natural product synthesis: organometallic additions to 4-methylpyrylium tetrafluoroborate
Richard J. K. Taylor Karl Hemming and Edna Faria De Medeiros
pg 2385; DOI:
10.1039/P19950002385
PDF
Intramolecular Diels–Alder reactions of the furan diene (IMDAF); rapid construction of highly functionalised isoquinoline skeletons
Tomas Hudlicky Gabor Butora Stephen P. Fearnley Andrew G. Gum P. J. Persichini III Michele R. Stabile and Joseph S. Merola
pg 2393; DOI:
10.1039/P19950002393
PDF
Biosynthesis of the dialkylmaleic anhydride-containing antibiotics, tautomycin and tautomycetin
Makoto Ubukata Xing-Chun Cheng Jun Uzawa and Kiyoshi Isono
pg 2399; DOI:
10.1039/P19950002399
PDF
Highly asymmetric Pummerer-type cyclization of chiral, non-racemic -amido sulfoxides
Yasuyuki Kita Norio Shibata Noriyuki Kawano Takashi Tohjo Chino Fujimori Keita Matsumoto and Shigekazu Fujita
pg 2405; DOI:
10.1039/P19950002405
PDF
Asymmetric aldol reactions of achiral 2-phenylsulfanyl aldehydes with small- and medium-sized carbocyclic rings: the synthesis of homochiral spirocyclic lactones, pyrrolidines and tetrahydrofurans
Kelly Chibale and Stuart Warren
pg 2411; DOI:
10.1039/P19950002411
PDF
Reactions of ethyl 2-acetyl-2-azabicyclo[2.2.1]hept-5-ene-3-carboxylate and 4-acetylamino-2-oxabicyclo[3.3.0]oct-7-en-3-one with some electrophiles
Michael B. Hursthouse K. M. Abdul Malik David E. Hibbs Stanley M. Roberts Amanda J. H. Seago Vladimir ik and Richard Storer
pg 2419; DOI:
10.1039/P19950002419
PDF
Synthesis and reactivity of iron carbonyl complexes of -silyl substituted ,-unsaturated ketones
Susan E. Gibson (née Thomas) and Gary J. Tustin
pg 2427; DOI:
10.1039/P19950002427
PDF
Reactivity of the carbonyl group in water. Generation of azomethine ylides from aqueous formaldehyde: Michael addition versus dipolar trapping
André Lubineau Giliane Bouchain and Yves Queneau
pg 2433; DOI:
10.1039/P19950002433
PDF
Ring-opening of N-tosyl aziridines by 2-lithiodithianes
William Howson Helen M. I. Osborn and Joseph Sweeney
pg 2439; DOI:
10.1039/P19950002439
PDF
Synthesis and sweet taste of optically active (–)-haematoxylin and of some ()-haematoxylin derivatives
Anna Arnoldi Angela Bassoli Gigliola Borgonovo and Lucio Merlini
pg 2447; DOI:
10.1039/P19950002447
PDF
Novel and unexpected one-pot synthesis of 7,7-dioxo-14-oxa-76-thiadibenzo[a,j]anthracene-2,12-disulfonic acid from -tetralone
M Fé de la Torre M Luisa Mussons César Raposo José Luis López Josefa Anaya M Cruz Caballero and Joaquín R. Morán
pg 2455; DOI:
10.1039/P19950002455
PDF
Substrate structure and incubation-parameter-dependent selectivities in chiral discrimination of galactopyranosides by -galactosidase hydrolysis
Barbara Werschkun Wilfried A. König Vladimír Ken and Joachim Thiem
pg 2459; DOI:
10.1039/P19950002459
PDF
Synthesis of imidazole 1-oxides from 1,2-diimines
Jesús Alcázar Mikael Begtrup and Antonio de la Hoz
pg 2467; DOI:
10.1039/P19950002467
PDF
-Substituted pyrrole-based silyl dienol ethers as -amino acid enolate equivalents: a versatile entry to racemic -substituted -amino acids
Franca Zanardi Lucia Battistini Gloria Rassu Mara Cornia and Giovanni Casiraghi
pg 2471; DOI:
10.1039/P19950002471
PDF
1,5-Asymmetric induction in reactions between aldehydes and [(4S)-5-(tert-butyldimethylsilyloxy)-4-hydroxypent-2-enyl](tributyl)-stannane promoted by tin(IV) chloride
Robert J. Maguire and Eric J. Thomas
pg 2477; DOI:
10.1039/P19950002477
PDF
Stereoselective synthesis of cis- and trans-2,6-disubstituted 5,6-dihydro-2H-pyrans based on 1,5-asymmetric induction in reactions between allylstannanes and aldehydes promoted by tin(IV) chloride
Robert J. Maguire and Eric J. Thomas
pg 2487; DOI:
10.1039/P19950002487
PDF
Ag+ Ion-selective lariat ethers: high pressure syntheses and cation recognition properties
Kiyoshi Matsumoto Masao Hashimoto Mitsuo Toda and Hiroshi Tsukube
pg 2497; DOI:
10.1039/P19950002497
PDF
Metallation of pyridine N-oxides and application to synthesis
Olivier Mongin Patrick Rocca Laurence Thomas-dit-Dumont François Trécourt Francis Marsais Alain Godard and Guy Quéguiner
pg 2503; DOI:
10.1039/P19950002503
PDF
Ozonolysis of (cyclohexa-1,4-dienyl)-L-alanine. An approach to the synthesis of new unnatural amino acids. X-Ray molecular structure of 2-hydroxy-7-methyl-3-phenylpyrazolo[1,5-a]pyrimidine
Gury Zvilichovsky and Vadim Gurvich
pg 2509; DOI:
10.1039/P19950002509
PDF
Photoinduced electron-transfer reactions of homonaphthoquinones with amine and arene donors
Hiroshi Moriwaki Takumi Oshima and Toshikazu Nagai
pg 2517; DOI:
10.1039/P19950002517
PDF
Conference diary

pg ixc; DOI:
10.1039/P19950000ixc
PDF

Issue 20


Front cover

pg X081; DOI:
10.1039/P199500FX081
PDF
Back cover

pg X083; DOI:
10.1039/P199500BX083
PDF
Journals bulletin

pg X085; DOI:
10.1039/P1995000X085
PDF
Contents pages

pg P219; DOI:
10.1039/P199500FP219
PDF
Back matter

pg P229; DOI:
10.1039/P199500BP229
PDF
Use of cyclodextrins to limit product inhibition of (S)-phenylalanine ammonia lyase
Christopher J. Easton Jason B. Harper and Stephen F. Lincoln
pg 2525; DOI:
10.1039/P19950002525
PDF
Oxidation of some prochiral 3-substituted cyclobutanones using monooxygenase enzymes: a single-step method for the synthesis of optically enriched 3-substituted -lactones
René Gagnon Gideon Grogan Esther Groussain Sandrine Pedragosa-Moreau Paul F. Richardson Stanley M. Roberts Andrew J. Willetts Véronique Alphand Jacques Lebreton and Roland Furstoss
pg 2527; DOI:
10.1039/P19950002527
PDF
Short synthetic approach towards the triindenotriphenylene (hemifullerene) system
G. Mehta G. V. Raghava Sharma (the late) M. A. Krishna Kumar T. V. Vedavyasa and E. D. Jemmis
pg 2529; DOI:
10.1039/P19950002529
PDF
Aryllead-mediated synthesis of linear 3-arylpyranocoumarins: synthesis of robustin and robustic acid
Dervilla M. X. Donnelly David J. Molloy John P. Reilly and Jean-Pierre Finet
pg 2531; DOI:
10.1039/P19950002531
PDF
Regio- and enantio-selective enolisations of cyclic ketones using chiral lithium amide bases
Kimberley Bambridge Barry P. Clark and Nigel S. Simpkins
pg 2535; DOI:
10.1039/P19950002535
PDF
Synthesis, X-ray structure, thermal stability and reactions of triaryl(3-oxoalkyl)bismuthonium salts
Yoshihiro Matano Nagao Azuma and Hitomi Suzuki
pg 2543; DOI:
10.1039/P19950002543
PDF
Steric acceleration of intramolecular oxime and hydrazone cycloadditions
Jane E. Bishop Katherine A. Flaxman Barry S. Orlek Peter G. Sammes and David J. Weller
pg 2551; DOI:
10.1039/P19950002551
PDF
Bis(hydroxyphenyloxazolinato)-titanium(IV) and -zirconium(IV) triflates as novel transition metal-based Lewis acids
Pier Giorgio Cozzi and Carlo Floriani
pg 2557; DOI:
10.1039/P19950002557
PDF
Benzazepine formation by the 1.7 electrocyclisations of diene-conjugated nitrile ylides: studies on relative rates of cyclisation via intramolecular competition reactions
Kevin E. Cullen and John T. Sharp
pg 2565; DOI:
10.1039/P19950002565
PDF
Synthesis of 17H-tetrabenzo[a,c,g,i]fluorene derivatives as chiral selectors for enantiomeric separation by HPLC on porous graphitised carbon
Jonathan K. Dutton John H. Knox Xavier Radisson Harold J. Ritchie and Robert Ramage
pg 2581; DOI:
10.1039/P19950002581
PDF
Synthesis of photoresponsive crown ethers having a phosphoric acid functional group as anionic cap and their selective complexing abilities toward alkali metal cations
Sadatoshi Akabori Yoshikazu Miura Noriko Yotsumoto Kiyoshi Uchida Masaru Kitano and Yoichi Habata
pg 2589; DOI:
10.1039/P19950002589
PDF
Synthesis of some -trichloromethyl-azines and -diazines
David Cartwright John R. Ferguson Thomas Giannopoulos George Varvounis and Basil J. Wakefield
pg 2595; DOI:
10.1039/P19950002595
PDF
Asymmetric formal total synthesis of (–)-swainsonine
Wei-Shan Zhou Wen-Ge Xie Zhi-Hui Lu and Xin-Fu Pan
pg 2599; DOI:
10.1039/P19950002599
PDF
Reaction of N-arylsulfonylaziridines with dimethylsulfoniumethoxycarbonyl methylide: regio- and stereo-selective synthesis of 1-arylsulfonyl-2-ethoxycarbonyl azetidines
Upender K. Nadir and Anjali Arora
pg 2605; DOI:
10.1039/P19950002605
PDF
Novel synthesis of 5,10,15,20-tetraarylporphyrins using high-valent transition metal salts
Ana Gradillas Carmen del Campo José V. Sinisterra and Emilio F. Llama
pg 2611; DOI:
10.1039/P19950002611
PDF
Atropisomer-selective ligand-coupling reactions of sulfoxides. X-Ray molecular and crystal structures for 2-({2-(4-chlorophenyl)naphtho[1,2-b]thiophen-3-yl}amino)-2-methylpropan-1-ol, 2-(2-hydroxy-1,1-dimethylethyl)-2,3-dihydronaphtho[2,1-d]isothiazol-3-one and (R)-(+)-2-bromo-1-(tert-butylsulfinyl)naphthalene
Robert W. Baker David C. R. Hockless Geoffrey R. Pocock Melvyn V. Sargent Brian W. Skelton Alexander N. Sobolev Edi Twiss (née Stanojevic) and Allan H. White
pg 2615; DOI:
10.1039/P19950002615
PDF
Lewis acid induced N-methyleneamine equivalents. Part 3. Addition of allyl nucleophiles to TiCl4-induced N-methyleneamine equivalents: synthesis of 1,2,3,4-tetrahydroquinolines and homoallylic anilines
Hyun-Joon Ha Young-Gil Ahn and Jung-Kyoon Chon
pg 2631; DOI:
10.1039/P19950002631
PDF
Photocycloaddition-cyclobutane rearrangement to spiro cyclopentanones: application in a formal synthesis of ()--cedrene
Debasis Patra and Subrata Ghosh
pg 2635; DOI:
10.1039/P19950002635
PDF
2-Azaallyl anions: key models for the elaboration of alkyl-, amino- and hydroxy-1,7-naphthyridine derivatives
Axel Couture Pierre Grandclaudon Cristian Simion and Patrice Woisel
pg 2643; DOI:
10.1039/P19950002643
PDF
Synthetic application of biotransformations: absolute stereochemistry and Diels–Alder reactions of the (1S,2R)-1,2-dihydroxycyclohexa-3,5-diene-1-carboxylic acid from Pseudomonas putida
Gareth N. Jenkins Douglas W. Ribbons David A. Widdowson Alexandra M. Z. Slawin and David J. Williams
pg 2647; DOI:
10.1039/P19950002647
PDF
ipso-vs. tele-Nucleophilic substitution by piperidine on isocolchicides and colchicides bearing an -leaving group
Marino Cavazza and Francesco Pietra
pg 2657; DOI:
10.1039/P19950002657
PDF
Synthesis and cycloaddition of 2,4-dihydropyrrolo[3,4-b]indoles
Arumugasamy Jeevanandam and Panayencheri C. Srinivasan
pg 2663; DOI:
10.1039/P19950002663
PDF
Conference diary

pg ixd; DOI:
10.1039/P19950000ixd
PDF

Issue 21


Front cover

pg X089; DOI:
10.1039/P199500FX089
PDF
Back cover

pg X091; DOI:
10.1039/P199500BX091
PDF
Contents pages

pg P231; DOI:
10.1039/P199500FP231
PDF
Stereoselective synthesis of 3--D-ribofuranosylpyrazole from 2,3-O-isopropylidene-D-ribose; a new route to pyrazole C-nucleosides
Anthony D. Rycroft Gurdial Singh and Richard H. Wightman
pg 2667; DOI:
10.1039/P19950002667
PDF
Samarium diiodide promoted coupling of thiophenecarbaldehydes
Shyh-Ming Yang and Jim-Min Fang
pg 2669; DOI:
10.1039/P19950002669
PDF
Enantioselective synthesis of -arylpropanoic acids
Philip C. Bulman Page Michael J. McKenzie and Derek R. Buckle
pg 2673; DOI:
10.1039/P19950002673
PDF
Facile synthesis of the key intermediate of EO 9 via the formation of the indole skeleton using the Nenitzescu reaction
Masahiko Kinugawa Hitoshi Arai Hiroshi Nishikawa Akihiko Sakaguchi Takehiro Ogasa Shinji Tomioka and Masaji Kasai
pg 2677; DOI:
10.1039/P19950002677
PDF
Facile retro-cycloaddition of adducts derived from steroidal 5,7-diene and 4-phenyl-1,2,4-triazoline-3,5-dione by diisobutylaluminium hydride
Fumihiro Kondo Misako Miyashita Katsuhiro Konno and Hiroaki Takayama
pg 2679; DOI:
10.1039/P19950002679
PDF
Preparation and direct observation by 19F NMR spectroscopy of 1-fluoro-1-lithioalkenes
Andrew Pelter Jaroslav Kvicala and David E. Parry
pg 2681; DOI:
10.1039/P19950002681
PDF
Novel synthesis of 3-chloromethylidene-2-ethoxy-1,25-oxaphospholan-2-ones catalysed by palladium(II)
Chunlin Ma Xiyan Lu and Yongxiang Ma
pg 2683; DOI:
10.1039/P19950002683
PDF
Active conformation of the inositol monophosphatase substrate, adenosine 2-phosphate: role of the ribofuranosyl O-atoms in chelating a second Mg2+ ion
Andrew G. Cole and David Gani
pg 2685; DOI:
10.1039/P19950002685
PDF
Probes for the position and mechanistic role of the second catalytic magnesium ion in the inositol monophosphatase reaction
Andrew G. Cole John Wilkie and David Gani
pg 2695; DOI:
10.1039/P19950002695
PDF
3-Dimensional interactions between inositol monophosphatase and its substrates, inhibitors and metal ion cofactors
John Wilkie Andrew G. Cole and David Gani
pg 2709; DOI:
10.1039/P19950002709
PDF
The lithiation of fluorinated benzenes and its dependence on solvent and temperature
Paul Leslie Coe Anthony John Waring and Thomas David Yarwood
pg 2729; DOI:
10.1039/P19950002729
PDF
Synthesis of 4-phenylpiperidines by tandem Wittig olefination–aza-Wittig rearrangement of 2-benzoylaziridines
Iain Coldham Alan J. Collis Roger J. Mould and Richard E. Rathmell
pg 2739; DOI:
10.1039/P19950002739
PDF
Synthesis of ()-aklavinone and ()-auramycinone via electron-deficient o-quinonoid pyrones
David W. Jones and Christopher J. Lock
pg 2747; DOI:
10.1039/P19950002747
PDF
LICKOR-Promoted 1,2-elimination in 1,1-dimethoxy-2-phenylethane and 1,1-dimethoxy-2-phenylpropane: synthesis of substituted enol ethers and alkynes
Annamaria Deagostino Mariella Mella Cristina Prandi and Paolo Venturello
pg 2757; DOI:
10.1039/P19950002757
PDF
Regio- and stereo-selective synthesis of trifluoromethylated isoxazolidines by 1,3-dipolar cycloaddition of 1,1,1-trifluoro-3-phenylsulfonylpropene with nitrones, and their conversion into trifluoromethylated syn-3-amino alcohols
Hiroyasu Tsuge Takashi Okano and Shoji Eguchi
pg 2761; DOI:
10.1039/P19950002761
PDF
Synthesis of some analogues of cytisine: unusual reduction pathways for tertiary nitro groups in sterically constrained molecules
Kristina J. Blackall David Hendry Robert J. Pryce and Stanley M. Roberts
pg 2767; DOI:
10.1039/P19950002767
PDF
Synthesis of 4-hydroxylamino-1-azabuta-1,3-dienes and their cyclization to 2-substituted pyrazole 1-oxides
Jesús Alcazar Inés Almena Mikael Begtrup and Antonio de la Hoz
pg 2773; DOI:
10.1039/P19950002773
PDF
Antitumour imidazotetrazines. Part 33. New syntheses of the antitumour drug temozolomide using masked methyl isocyanates
Yongfeng Wang Malcolm F. G. Stevens William T. Thomson and Bruce P. Shutts
pg 2783; DOI:
10.1039/P19950002783
PDF
Ligand coupling and neighbouring-group effects in the alkaline hydrolysis of arylphosphonium salts: new stable tetraarylphosphonium benzimidazolate betaines
David W. Allen and Peter Benke
pg 2789; DOI:
10.1039/P19950002789
PDF
Synthesis of 1,6-diethynylcyclohepta-1,3,5-triene and its oxidative coupling to dimethano-bridged octadehydro[20]annulene and trimethano-bridged dodecadehydro[30]annulene
Jro Ojima Tomoyo Daimon Naoki Hiraiwa Hiroyuki Higuchi Masako Ueno and Gaku Yamamoto
pg 2795; DOI:
10.1039/P19950002795
PDF
Diastereoselectivity and assignment of absolute stereochemistry in the aza-Diels–Alder reaction of a sulfonylimino acetate with 1-methoxy-3-trimethylsilyloxybuta-1,3-diene
Andrew K. McFarlane Gareth Thomas and Andrew Whiting
pg 2803; DOI:
10.1039/P19950002803
PDF
Corrigendum
A. V. Nikolaev T. J. Rutherford M. A. J. Ferguson and J. S. Brimacombe
pg 2809; DOI:
10.1039/P19950002809
PDF
Conference diary

pg ixe; DOI:
10.1039/P19950000ixe
PDF

Issue 22


Front cover

pg X093; DOI:
10.1039/P199500FX093
PDF
Back cover

pg X095; DOI:
10.1039/P199500BX095
PDF
Contents pages

pg P241; DOI:
10.1039/P199500FP241
PDF
Assembly of bicyclo[2.2.1]heptane derivatives by two types of domino reaction
Masataka Ihara Shuichi Suzuki Yuji Tokunaga and Keiichiro Fukumoto
pg 2811; DOI:
10.1039/P19950002811
PDF
Cyclopenta[a]phenalen-9(8H)-one: an extended phenalenone system
Yoshikazu Sugihara Reiko Hashimoto Hitoshi Fujita Noritaka Abe Hiromasa Yamamoto Takashi Sugimura and Ichiro Murata
pg 2813; DOI:
10.1039/P19950002813
PDF
Characterization of an imidazolium compound formed by reaction of methylglyoxal and N-hippuryllysine
Elisabeth Brinkmann Kevin J. Wells-Knecht Suzanne R. Thorpe and John W. Baynes
pg 2817; DOI:
10.1039/P19950002817
PDF
Studies in the cycloproparene series; heterocyclic substituted methylidenecyclopropa[b]naphthalenes
Brian Halton Mark J. Cooney Tim W. Davey Grant S. Forman Qi Lu Roland Boese Dieter Bläser and Andreas H. Maulitz
pg 2819; DOI:
10.1039/P19950002819
PDF
Mechanistic studies of a Pummerer-type reaction in acyclic and rigid cyclic sulfoxides induced by ketene tert-butyldimethylsilyl methyl acetal
Yasuyuki Kita Norio Shibata Naoki Yoshida Noriyuki Kawano Chino Fujimori Naoki Yoshikawa and Shigekazu Fujita
pg 2829; DOI:
10.1039/P19950002829
PDF
New route to 1-formylalkylphosphonates using diethyl trichloromethylphosphonate as a precursor
Yannick Zanella Sylvie Berté-Verrando Rachel Dizière and Philippe Savignac
pg 2835; DOI:
10.1039/P19950002835
PDF
Stereochemical and mechanistic studies on the formation of the 3-oxoindolizidine skeleton from ornithine derivatives
M José Domínguez M Teresa García-López Rosario Herranz Mercedes Martín-Martínez and Rosario González-Muñiz
pg 2839; DOI:
10.1039/P19950002839
PDF
Rearrangement of 1-phenyl-3,4-dihydro-1H-2-benzothiopyranium 2-methylides
Toru Tanzawa Naohiro Shirai Yoshiro Sato Keiichiro Hatano and Yukihisa Kurono
pg 2845; DOI:
10.1039/P19950002845
PDF
Highly stereocontrolled total synthesis of (+)-bengamide E
Chisato Mukai Sameh M. Moharram Osamu Kataoka and Miyoji Hanaoka
pg 2849; DOI:
10.1039/P19950002849
PDF
Synthesis of arizonin C1
Margaret A. Brimble Sara J. Phythian and Hishani Prabaharan
pg 2855; DOI:
10.1039/P19950002855
PDF
Syntheses of 6-hydroxyshikimic acid and its derivatives
A. John Blacker R. John Booth Gareth M. Davies and James K. Sutherland
pg 2861; DOI:
10.1039/P19950002861
PDF
Synthesis of chiral diferrocenyl dichalcogenides and their application to asymmetric nucleophilic ring opening of meso-epoxides
Yoshiaki Nishibayashi Jai Deo Singh Shin-ichi Fukuzawa and Sakae Uemura
pg 2871; DOI:
10.1039/P19950002871
PDF
(2R, 3S)- and (2S, 3R)-2-Benzyl-3,4-epoxybutanoic acid as highly efficient and fast acting pseudomechanism-based inactivators for carboxypeptidase a: design, asymmetric synthesis and inhibitory kinetics
Soo Suk Lee Zhi-Hong Li Dong Ha Lee and Dong H. Kim
pg 2877; DOI:
10.1039/P19950002877
PDF
Synthesis of aliphatic O-dimannosyl amino acid building blocks for solid-phase assembly of glycopeptide libraries
Henrik Franzyk Morten Meldal Hans Paulsen and Klaus Bock
pg 2883; DOI:
10.1039/P19950002883
PDF
Activity and enantioselectivity of serine proteases in transesterification reactions in organic media
Jaap Broos Johan F. J. Engbersen Inna K. Sakodinskaya Willem Verboom and David N. Reinhoudt
pg 2899; DOI:
10.1039/P19950002899
PDF
Heterocyclizations of 3-trifluoroacetyl substituted lactams with cyclic 1,3-bis-nucleophiles
Jean-Philippe Bouillon Zdenek Janousek Heinz G. Viehe Bernard Tinant and Jean-Paul Declercq
pg 2907; DOI:
10.1039/P19950002907
PDF
Diastereoselective allylation of chiral sulfinyl-substituted thiophenecarbaldehydes with a Lewis acid
Yoshitsugu Arai Atsuko Suzuki Tsutomu Masuda Yukio Masaki and Motoo Shiro
pg 2913; DOI:
10.1039/P19950002913
PDF
trans-Fused crown ethers from 2,5-O-methylene-D-mannitol: synthesis, X-ray diffraction structure and full nuclear magnetic resonance spectroscopic data of 1,6-diazido-1,6-dideoxy-2,5-O-methylene-3,4-O-naphthalene-2,3-diylbis(oxyethyleneoxyethylene)-D-mannitol and 3,4-di-O-acetyl-1,6-diazido-1,6-dideoxy-2,5-O-methylene-D-mannitol
Mostafa Nazhaoui Jean-Pierre A. Joly Bertrand J. Jean-Claude Valerio Del Duca André Aubry and Mohammed Boubouh
pg 2919; DOI:
10.1039/P19950002919
PDF
(Z)-Heptadec-8-enylboronic acid: a potential lipase inhibitor
Valeri Martichonok and J. Bryan Jones
pg 2927; DOI:
10.1039/P19950002927
PDF
Photochemistry of the nitrogen–thiocarbonyl systems. Part. 24. Photoreactions of thiobenzamide with various substituted furans: regioselective -benzoylation and transformation of furans to other aromatic compounds
Kazuaki Oda Hisao Tsujita Kosei Ohno and Minoru Machida
pg 2931; DOI:
10.1039/P19950002931
PDF
Diacetylenic sterols: new potentially photopolymerizable lipids
Catherine Vilchèze and Robert Bittman
pg 2937; DOI:
10.1039/P19950002937
PDF
Preparation of thiazolocarbazoles via the Fischer indole synthesis
Laurent Martarello Delphine Joseph and Gilbert Kirsch
pg 2941; DOI:
10.1039/P19950002941
PDF
Reactivity of cyclic arsenites and phosphites: X-ray structures of bis(5,5-dimethyl-1,3,2-dioxarsenan-2-yl) ether and bis(2,4,8,10-tetra-tert-butyl-12H-dibenzo [d,g][1,3,2]dioxarsenocin-6-yl) ether
Musa A. Said K. C. Kumara Swamy M. Veith and V. Huch
pg 2945; DOI:
10.1039/P19950002945
PDF
Conference diary

pg ixf; DOI:
10.1039/P19950000ixf
PDF

Issue 23


Front cover

pg X097; DOI:
10.1039/P199500FX097
PDF
Back cover

pg X099; DOI:
10.1039/P199500BX099
PDF
Contents pages

pg P251; DOI:
10.1039/P199500FP251
PDF
Back matter

pg P259; DOI:
10.1039/P199500BP259
PDF
Alkoxycarbonyl groups transfer to amines by the N,N-dibenzyl-and N,N-di-tert-butyl-carbamates of cyclic thioureas
Noboru Matsumura Akiko Noguchi Aya Kitayoshi and Hiroo Inoue
pg 2953; DOI:
10.1039/P19950002953
PDF
Facile and stereospecific synthesis of 1,1-dihalogenoalk-1-enes from 1-halogenoalk-1-ynes by hydroboration
Yuzuru Masuda Toshihiro Suyama Miki Murata and Shinji Watanabe
pg 2955; DOI:
10.1039/P19950002955
PDF
Novel stereoselective incorporation and hydrolysis of long-chain amino-acid substrates by vesicular membrane systems which include tri- or tetra-peptide catalysts
Katsutoshi Ohkubo Kenji Urabe Junji Yamamoto Takashi Sagawa and Satoshi Usui
pg 2957; DOI:
10.1039/P19950002957
PDF
Kinetic resolution of alcohols in an asymmetric mitsunobu reaction using chiral nonracemic 1,3,2-dioxaphosphepanes
Ron Hulst Arjan van Basten Kevin Fitzpatrick and Richard M. Kellogg
pg 2961; DOI:
10.1039/P19950002961
PDF
Regiospecific synthesis of 4-fluoro-4,3-keto steroids using caesium fluoroxysulfate
Harold F. Hodson David J. Madge and David A. Widdowson
pg 2965; DOI:
10.1039/P19950002965
PDF
Biotransformation of -unsaturated carbonyl compounds: sulfides, sulfoxides, sulfones, nitriles and esters by yeast species: carbonyl group and carbon–carbon double bond reduction
Surinder Koul David H. G. Crout William Errington and Jiri Tax
pg 2969; DOI:
10.1039/P19950002969
PDF
New entry to a cis-fused bicyclic ring system by a [2,3]sigmatropic rearrangement via cyclic allylsulfonium ylides. Synthesis of the cis-2-oxa-9-vinyldecalin skeleton
Fusao Kido Toshiya Abiko and Michiharu Kato
pg 2989; DOI:
10.1039/P19950002989
PDF
Highly regioselective access to 7-substituted 1,4,7,10-tetraazacyclododecane-1-carbaldehyde derivatives: synthetic aspects and NMR elucidation of the structures. X-Ray crystal structures of 7-triphenylmethyl-1,4,7,10-tetraazacyclododecane-1-carbaldehyde and 7-triphenylmethyloctahydro-5H,9bH-2a,4a,7,9a-tetraazacycloocta [cd] pentalene
Pier Lucio Anelli Luisella Calabi Paolo Dapporto Marcella Murru Lino Paleari Paola Paoli Fulvio Uggeri Sandra Verona and Mario Virtuani
pg 2995; DOI:
10.1039/P19950002995
PDF
Oligomeric flavanoids. Part 19. Reductive cleavage of the interflavanyl bond in proanthocyanidins
Petrus J. Steynberg Jan P. Steynberg Barend C. B. Bezuidenhoudt and Daneel Ferreira
pg 3005; DOI:
10.1039/P19950003005
PDF
New, short synthesis of arylnaphthofuranone lignans based on reactions of o-aroylbenzyllithiums with furan-2(5H)-one
Kazuhiro Kobayashi Junsuke Tokimatsu Kouji Maeda Osamu Morikawa and Hisatoshi Konishi
pg 3013; DOI:
10.1039/P19950003013
PDF
Solid-phase synthesis of a fucosylated glycopeptide of human factor IX with a fucose--(1O)-serine linkage
Stefan Peters Todd L. Lowary Ole Hindsgaul Morten Meldal and Klaus Bock
pg 3017; DOI:
10.1039/P19950003017
PDF
Simple and efficient strategy for making -(16)-linked galactooligosaccharides using naked galactopyranosides as acceptors
Ravindranathan K. P. Kartha Makoto Kiso Akira Hasegawa and Harold J. Jennings
pg 3023; DOI:
10.1039/P19950003023
PDF
Synthesis and properties of dimethano-bridged tetradehydro[21]-, -[23]- and -[25]annulenones
Jro Ojima Naoki Hiraiwa Shiro Kondo Kaori Asano Chiaki Sakon Hiroyuki Higuchi Katsuya Inoue and Gaku Yamamoto
pg 3027; DOI:
10.1039/P19950003027
PDF
Biomimetic iron porphyrin-catalysed oxidation of cyclopenta [a] phenanthrenones
Grahame J. Harden and Maurice M. Coombs
pg 3037; DOI:
10.1039/P19950003037
PDF
Synthesis and reactions of 5-benzylidene-2-phenyl-4,5-dihydro-1,3-oxazol-4-ones
Yennu Santosh Laxmi and Divi Sarangapani Iyengar
pg 3043; DOI:
10.1039/P19950003043
PDF
Corrigendum
Vijay Nair and Jessy Mathew
pg 3047; DOI:
10.1039/P19950003047
PDF
Conference diary

pg viin; DOI:
10.1039/P1995000viin
PDF

Issue 24


Front cover

pg X101; DOI:
10.1039/P199500FX101
PDF
Back cover

pg X103; DOI:
10.1039/P199500BX103
PDF
Contents pages

pg P261; DOI:
10.1039/P199500FP261
PDF
Unimolecular chain transfer (UMCT) reactions: concepts, preliminary results with silicon hydrides, and future potential
Dennis P. Curran Jinyou Xu and Edoardo Lazzarini
pg 3049; DOI:
10.1039/P19950003049
PDF
Giese-type radical addition reactions to an acceptor that functions by a unimolecular chain transfer reaction of a silicon hydride
Dennis P. Curran and Jinyou Xu
pg 3061; DOI:
10.1039/P19950003061
PDF
Design of new phosphonium salt host compounds
Fumio Toda Koichi Tanaka and Hirotoshi Sawada
pg 3065; DOI:
10.1039/P19950003065
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Studies on the stereoselectivity of osmylation of cis-bicyclo [3.3.0]-oct-6-enes
Nigel Broom Peter J. O'Hanlon Thomas J. Simpson Rosamund Stephen and Christine L. Willis
pg 3067; DOI:
10.1039/P19950003067
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Synthesis of enterochelin
Henry J. Rogers
pg 3073; DOI:
10.1039/P19950003073
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Aminolysis and alkaline hydrolysis of protected 1-hydroxybenzo-triazol-1-yl esters of adenosine 5-phosphorothioate and -phosphorodithioate
Colin B. Reese Louise H. K. Shek and Zhengyun Zhao
pg 3077; DOI:
10.1039/P19950003077
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Synthesis of cyclocholate-capped porphyrins
Richard P. Bonar-Law and Jeremy K. M. Sanders
pg 3085; DOI:
10.1039/P19950003085
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Photochemical reaction of 1-(o-methylaryl)-2,2-dimethyl 1,3-diketones in the presence of oxygen
Michikazu Yoshioka Kaori Nishizawa Johji Suzuki Yasuhiro Iwata Shigekazu Kumakura and Tadashi Hasegawa
pg 3097; DOI:
10.1039/P19950003097
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Three positional isomers of substituted triphenylmethanes from reactions of trityl anion with 1-acyl-2,2-dimethylaziridines
Jürgen Werry Pen-Yuan Lin Petros Assithianakis and Helmut Stamm
pg 3103; DOI:
10.1039/P19950003103
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Sesqui- and di-terpene biosynthesis from 13C labelled acetate and mevalonate in cultured cells of Heteroscyphus planus
Kensuke Nabeta Takehiro Ishikawa and Hiroshi Okuyama
pg 3111; DOI:
10.1039/P19950003111
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Synthesis and oxidative behaviour of reduced indeno[1,2-b]quinoxalines and benzo[b]phenazines
David W. Brown Mary F. Mahon Aleyamma Ninan and Malcolm Sainsbury
pg 3117; DOI:
10.1039/P19950003117
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New route to amino[2H2]methylphosphonic acid via bis(trifluoroethyl) phosphonate transesterification
Sylvie Berté-Verrando Rachel Dizière Mohammad Samadi and Philippe Savignac
pg 3125; DOI:
10.1039/P19950003125
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Conversions of 2-aminopyridines into 5-substituted derivatives mediated by 1-hydroxymethylbenzotriazole
Alan R. Katritzky Saad El-Zemity and Hengyuan Lang
pg 3129; DOI:
10.1039/P19950003129
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Synthesis of the Calophyllum coumarins. Part 2
Christopher J. Palmer and Jonathan L. Josephs
pg 3135; DOI:
10.1039/P19950003135
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Conference diary

pg viio; DOI:
10.1039/P1995000viio
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